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2,2'-Dithiosalicylic acid
Cas No: 119-80-2
No Data No Data / Zouping Mingxing Chemical Co.,Ltd. Contact Supplier
2,2'-Dithiosalicylic acid Manufacturer/High quality/Best price/In stock
Cas No: 119-80-2
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality 2-Hydroxybenzenecarbothioic Acid supplier in China
Cas No: 119-80-2
No Data No Data Metric Ton/Day Simagchem Corporation Contact Supplier
2,2'-Dithiosalicylic acid
Cas No: 119-80-2
USD $ 11.0-16.0 / Kilogram 1 Kilogram 10 Metric Ton/Day Hebei yanxi chemical co.,LTD. Contact Supplier
CAS 119-80-2 2,2'-Dithiosalicylic acid
Cas No: 119-80-2
USD $ 20.0-30.0 / Gram 10 Gram 200 Metric Ton/Year Jinan Finer Chemical Co., Ltd Contact Supplier
2,2'-Dithiosalicylic acid -- CHemwill
Cas No: 119-80-2
USD $ 1.0-1.0 / Metric Ton 1 Metric Ton 5 Metric Ton/Day Chemwill Asia Co., Ltd. Contact Supplier
2,2'-Dithiosalicylic acid
Cas No: 119-80-2
No Data 1 Kilogram 20 Metric Ton/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier
2,2′-dithiodibenzoic acid CAS:119-80-2
Cas No: 119-80-2
USD $ 0.32-0.98 / Gram 1 Gram 1 Metric Ton/Day WUHAN MULEI NEW MATERIAL CO., LTD Contact Supplier
2-[(2-carboxylatophenyl)disulfanyl]benzoate
Cas No: 119-80-2
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
2,2'-Dithiodibenzoic acid
Cas No: 119-80-2
USD $ 5.0-5.0 / Kilogram 1 Kilogram 1000 Kilogram/Month Enke Pharma-tech Co.,Ltd. (Cangzhou, China ) Contact Supplier

119-80-2 Usage

Uses

An organosulfur compound produced from dibenzothiophene metabolites that is in turn biodegraded into transient metabolites such as benzoic acid. Used in the preparation of a new class of anti-HIV-1 agents.

Chemical Properties

brown powder

119-80-2 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
USP (1659001)  ThimerosalRelatedCompoundA  United States Pharmacopeia (USP) Reference Standard 119-80-2 1659001-50MG 14,500.98CNY Detail
Alfa Aesar (L04213)  2,2'-Dithiosalicylic acid, 96%    119-80-2 500g 942.0CNY Detail
Alfa Aesar (L04213)  2,2'-Dithiosalicylic acid, 96%    119-80-2 100g 259.0CNY Detail

119-80-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 2,2-Dithiosalicylic Acid

1.2 Other means of identification

Product number -
Other names Dithiosalicylic Acid

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:119-80-2 SDS

119-80-2Synthetic route

Thiosalicylic acid
147-93-3

Thiosalicylic acid

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With xenon difluoride In dichloromethane at 25℃;99%
With 1-oxa-2-azaspiro[2.5]octane In toluene99%
With polyvinylpolypyrrolidonium tribromide In ethanol at 20℃; for 1.5h; Green chemistry;99%
2-Iodobenzoic acid
88-67-5

2-Iodobenzoic acid

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With nickel(II) chloride hexahydrate; morpholinium morpholine-1-carbodithioate; potassium hydroxide In water; ethylene glycol; N,N-dimethyl-formamide at 130℃;96%
With potassium sulfide; nickel(II) chloride hexahydrate; acetylacetone; potassium hydroxide In water; N,N-dimethyl-formamide at 110℃; for 24h;95%
2-bromobenzoic-acid
88-65-3

2-bromobenzoic-acid

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With indium(III) oxide; ammonia; water; sulfur In ethanol at 60℃; Green chemistry;82%
With copper(l) iodide; tetra(n-butyl)ammonium hydroxide; sulfur In water at 80℃; for 48h; Inert atmosphere; Sealed tube; chemoselective reaction;
Benzo[b]thiophene
95-15-8

Benzo[b]thiophene

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With ozone; acetic acid at 16.84℃;26.7%
dibenzothiophene
132-65-0

dibenzothiophene

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With ozone; acetic acid at 16.84℃;14%
2,2'-dithiodibenzoic acid dichloride
19602-82-5

2,2'-dithiodibenzoic acid dichloride

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
bei laengerem Liegen an feuchter Luft;
benzo-[b]thiophene-2,3-dione
493-57-2

benzo-[b]thiophene-2,3-dione

A

1,2-benzisothiazole-3-carboxamide
16807-21-9

1,2-benzisothiazole-3-carboxamide

B

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With ammonium hydroxide; dihydrogen peroxide
3H-1,2-benzodithiol-3-one
1677-27-6

3H-1,2-benzodithiol-3-one

sodium ethanolate
141-52-6

sodium ethanolate

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

3H-1,2-benzodithiol-3-one
1677-27-6

3H-1,2-benzodithiol-3-one

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With sodium ethanolate
3H-1,2-benzodithiole-3-thione
3354-42-5

3H-1,2-benzodithiole-3-thione

furan-2,3,5(4H)-trione pyridine (1:1)

furan-2,3,5(4H)-trione pyridine (1:1)

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

3H-1,2-benzodithiole-3-thione
3354-42-5

3H-1,2-benzodithiole-3-thione

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With alkali
With ethanol; sodium
4-chloro-3,5-diiodo-pyridine
13993-58-3

4-chloro-3,5-diiodo-pyridine

ethanol
64-17-5

ethanol

sodium ethanolate
141-52-6

sodium ethanolate

Thiosalicylic acid
147-93-3

Thiosalicylic acid

A

4-hydroxy-3,5-diiodopyridine
7153-08-4

4-hydroxy-3,5-diiodopyridine

B

4-ethoxy-3,5-diiodopyridine

4-ethoxy-3,5-diiodopyridine

C

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

D

2-(3,5-diiodo-[4]pyridylmercapto)-benzoic acid

2-(3,5-diiodo-[4]pyridylmercapto)-benzoic acid

1-thioflavone
784-62-3

1-thioflavone

sodium ethanolate
141-52-6

sodium ethanolate

A

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

B

1-(2-mercaptophenyl)ethan-1-one
26824-02-2

1-(2-mercaptophenyl)ethan-1-one

C

Thiosalicylic acid
147-93-3

Thiosalicylic acid

D

acetophenone
98-86-2

acetophenone

o-Carboxybenzenediazonium
17333-86-7

o-Carboxybenzenediazonium

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With sodium disulfide
With sodium disulfide
1-methyl-4-nitrosobenzene
623-11-0

1-methyl-4-nitrosobenzene

2-[(2-oxo-2-phenylethyl)thio]-benzoic acid
25803-71-8

2-[(2-oxo-2-phenylethyl)thio]-benzoic acid

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

o-(hydroxysulfinyl)benzoic acid
13165-80-5

o-(hydroxysulfinyl)benzoic acid

A

2-sulfobenzoic acid
632-25-7

2-sulfobenzoic acid

B

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

o-(hydroxysulfinyl)benzoic acid
13165-80-5

o-(hydroxysulfinyl)benzoic acid

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With hydrogenchloride; water; tin(ll) chloride
anthranilic acid
118-92-3

anthranilic acid

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

n-butyllithium
109-72-8, 29786-93-4

n-butyllithium

diethyl ether
60-29-7

diethyl ether

thiophenol
108-98-5

thiophenol

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
anschliessendes Behandeln mit festem CO2;
(Z)-2-bromo-1,3-diphenylprop-2-en-1-one
32147-20-9

(Z)-2-bromo-1,3-diphenylprop-2-en-1-one

Thiosalicylic acid
147-93-3

Thiosalicylic acid

A

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

B

2-(1-benzoyl-2-phenyl-vinylmercapto)-benzoic acid

2-(1-benzoyl-2-phenyl-vinylmercapto)-benzoic acid

Conditions
ConditionsYield
With ethanol; sodium carbonate; acetone
Thiosalicylic acid
147-93-3

Thiosalicylic acid

Bromoacetaldehyde diethyl acetal
2032-35-1

Bromoacetaldehyde diethyl acetal

A

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

B

2-(2,2-diethoxy-ethylsulfanyl)-benzoic acid

2-(2,2-diethoxy-ethylsulfanyl)-benzoic acid

Conditions
ConditionsYield
With ethanol; sodium acetate
n-butyllithium
109-72-8, 29786-93-4

n-butyllithium

diethyl ether
60-29-7

diethyl ether

diphenyldisulfane
882-33-7

diphenyldisulfane

A

(n-butylthio)benzene
1126-80-3

(n-butylthio)benzene

B

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
anschliessendes Behandeln mit festem CO2;
potassium thioacyanate
333-20-0

potassium thioacyanate

2-bromobenzoic-acid
88-65-3

2-bromobenzoic-acid

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With sodium hydroxide; copper
benzo[d]-1,3-oxathiin-4-one 1-oxide
36665-23-3

benzo[d]-1,3-oxathiin-4-one 1-oxide

A

formaldehyd
50-00-0

formaldehyd

B

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
In dimethylsulfoxide-d6 at 110℃; for 10h;
carbon dioxide
124-38-9

carbon dioxide

thiophenol
108-98-5

thiophenol

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With n-butyllithium 1.) hexane, r.t., overnight, 2.) r.t.; Yield given. Multistep reaction;
ortho-chlorobenzoic acid
118-91-2

ortho-chlorobenzoic acid

A

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

B

Thiosalicylic acid
147-93-3

Thiosalicylic acid

C

benzoic acid
65-85-0

benzoic acid

D

salicylic acid
69-72-7

salicylic acid

Conditions
ConditionsYield
With sulfur In melt at 270℃; Product distribution; effect of various molten salts, amount of sulfur, molar ratio of sulfur to molten salts, composition of molten salt and various mercaptylation agents;
carbon dioxide
124-38-9

carbon dioxide

Ethyl phenyl sulfide
622-38-8

Ethyl phenyl sulfide

Dipropyl disulfide
629-19-6

Dipropyl disulfide

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Conditions
ConditionsYield
With hydrogenchloride; n-butyllithium Yield given. Multistep reaction;
hydrogenchloride
7647-01-0

hydrogenchloride

1,1-dioxo-2,3-dihydro-1λ6-benzo[e][1,2,3]thiadiazin-4-one-hydrazone
1012-97-1

1,1-dioxo-2,3-dihydro-1λ6-benzo[e][1,2,3]thiadiazin-4-one-hydrazone

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

3H-1,2-benzodithiole-3-thione
3354-42-5

3H-1,2-benzodithiole-3-thione

natrium carbonate

natrium carbonate

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

methanol
67-56-1

methanol

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

bis[2-(methoxycarbonyl)phenyl]disulfide
5459-63-2

bis[2-(methoxycarbonyl)phenyl]disulfide

Conditions
ConditionsYield
With triethylamine for 18h;100%
Stage #1: 2,2'-dithiobenzoic acid With thionyl chloride for 2h; Reflux;
Stage #2: methanol With triethylamine for 2h; Reflux;
92%
With sulfuric acid for 24h; Reflux;91%
4-Chlorophenoxyacetic acid
122-88-3

4-Chlorophenoxyacetic acid

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

(1-chloro-9-oxo-9H-thioxanthen-4-yloxy)-acetic acid

(1-chloro-9-oxo-9H-thioxanthen-4-yloxy)-acetic acid

Conditions
ConditionsYield
99.5%
With sulfuric acid at 10 - 40℃; for 4 - 5h;73.8%
With sulfuric acid at -5 - 50℃; for 58h;53.8%
With sulfuric acid at -5 - 50℃; for 58h;
With sulfuric acid at 20℃; for 2h;
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

4-chloro-phenol
106-48-9

4-chloro-phenol

1-chloro-4-hydroxy-9H-thioxanthen-9-one
59803-22-4

1-chloro-4-hydroxy-9H-thioxanthen-9-one

Conditions
ConditionsYield
With sulfuric acid at -5 - 70℃; for 21h;99%
Stage #1: 2,2'-dithiobenzoic acid With sulfuric acid In water for 0.5h;
Stage #2: 4-chloro-phenol In water at 40 - 100℃; for 5h;
77.9%
In sulfuric acid69.7%
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

2-chlorosulfenylbenzoyl chloride
3950-02-5

2-chlorosulfenylbenzoyl chloride

Conditions
ConditionsYield
With chlorine; sulfur In 1,1,2,2-tetrachloroethylene at 70℃; Temperature; Solvent;99%
Stage #1: 2,2'-dithiobenzoic acid With thionyl chloride; 1-methyl-pyrrolidin-2-one at 80℃; Heating / reflux;
Stage #2: With sulfuryl dichloride at 50℃; for 0.5h;
93%
With thionyl chloride; chlorine; N,N-dimethyl-formamide 1.) 1,2-dichloroethane, reflux, 1 h, 2.) 10 deg C, 20 min; Multistep reaction;
Isopropylbenzene
98-82-8

Isopropylbenzene

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

2-isopropyl-9H-thioxanthen-9-one
5495-84-1

2-isopropyl-9H-thioxanthen-9-one

Conditions
ConditionsYield
With sulfuric acid at 20℃; for 0.5h;99%
With methanesulfonic acid; zinc In chlorobenzene at 115℃;89.5%
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

2,2'-dithiodibenzoic acid dichloride
19602-82-5

2,2'-dithiodibenzoic acid dichloride

Conditions
ConditionsYield
With thionyl chloride In N,N-dimethyl-formamide; toluene at 82℃; for 20h;97%
With thionyl chloride In N,N-dimethyl-formamide for 4h; Reflux;95%
With thionyl chloride; N,N-dimethyl-formamide In toluene at 82℃; for 20h;91.3%
indole
120-72-9

indole

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

2-((1H-indol-3-yl)thio)benzoic acid
81471-22-9

2-((1H-indol-3-yl)thio)benzoic acid

Conditions
ConditionsYield
With sodium hydroxide In water; isopropyl alcohol at 130℃; for 48h; Reagent/catalyst; Solvent; Temperature; Green chemistry;95%
Stage #1: 2,2'-dithiobenzoic acid With ammonium peroxydisulfate In methanol at 70℃; for 3h;
Stage #2: indole In methanol at 20 - 70℃;
46%
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

3H-1,2-benzodithiole-3-thione
3354-42-5

3H-1,2-benzodithiole-3-thione

Conditions
ConditionsYield
With tetraphosphorus decasulfide In 1,4-dioxane for 48h; Inert atmosphere; Reflux;93%
With phosphorous (V) sulfide; xylene
With Lawessons reagent In benzene Heating; Yield given;
With tetraphosphorus decasulfide In pyridine for 1h; Heating;
With pyridine; tetraphosphorus decasulfide
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

C14H10O5S2

C14H10O5S2

Conditions
ConditionsYield
With dihydrogen peroxide In neat (no solvent) at 20℃; for 0.5h; Reagent/catalyst; chemoselective reaction;92%
With dihydrogen peroxide In neat (no solvent) at 20℃; for 0.5h; Reagent/catalyst; Green chemistry;92%
4-hydroxy[1]benzopyran-2-one
1076-38-6

4-hydroxy[1]benzopyran-2-one

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

3-(2-carboxyphenylthio)-4-hydroxy-coumarin

3-(2-carboxyphenylthio)-4-hydroxy-coumarin

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 90 - 95℃; for 5h; Substitution;91%
6-fluoro-1H-indole
399-51-9

6-fluoro-1H-indole

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

6-fluoro-3-[(2-carboxyphenyl)thio]-1H-indole

6-fluoro-3-[(2-carboxyphenyl)thio]-1H-indole

Conditions
ConditionsYield
With sodium hydroxide In water; isopropyl alcohol at 130℃; Green chemistry;91%
m-diethylbenzene
141-93-5

m-diethylbenzene

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

2,4‐diethyl‐9H‐thioxanthene‐9‐one
82799-44-8

2,4‐diethyl‐9H‐thioxanthene‐9‐one

Conditions
ConditionsYield
With sulfuric acid at 0 - 65℃; for 6h; Reagent/catalyst;90.2%
With aluminum oxide; iron; toluene-4-sulfonic acid at 130℃; Reagent/catalyst;89%
1-hydroxy-pyrrolidine-2,5-dione
6066-82-6

1-hydroxy-pyrrolidine-2,5-dione

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

N,N'-disuccinimidyl-2,2'-dithiosalicylate
497262-13-2

N,N'-disuccinimidyl-2,2'-dithiosalicylate

Conditions
ConditionsYield
With diisopropyl-carbodiimide In tetrahydrofuran; isopropyl alcohol at 20℃; for 4h;89%
With diisopropyl-carbodiimide In tetrahydrofuran; isopropyl alcohol at 25℃; for 4h;89%
With diisopropyl-carbodiimide In tetrahydrofuran; isopropyl alcohol at 25℃;
5-fluoro-1H-indole
399-52-0

5-fluoro-1H-indole

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

C15H10FNO2S

C15H10FNO2S

Conditions
ConditionsYield
With sodium hydroxide In water; isopropyl alcohol at 130℃; Green chemistry;89%
4-hydroxy-1-methyl-2(1H)-quinolone
1677-46-9

4-hydroxy-1-methyl-2(1H)-quinolone

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

3-(2-carboxyphenylthio)-4-hydroxy-1-methyl-2(1H)-quinolone

3-(2-carboxyphenylthio)-4-hydroxy-1-methyl-2(1H)-quinolone

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 90 - 95℃; for 5h; Substitution;87%
5-methoxylindole
1006-94-6

5-methoxylindole

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

5-methoxyl-3-[(2-carboxyphenyl)thio]-1H-indole

5-methoxyl-3-[(2-carboxyphenyl)thio]-1H-indole

Conditions
ConditionsYield
With sodium hydroxide In water; isopropyl alcohol at 130℃; Green chemistry;86%
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

Thiosalicylic acid
147-93-3

Thiosalicylic acid

Conditions
ConditionsYield
With hydrogenchloride; hydrogen iodide; hypophosphorous acid for 3h; Heating;85%
With hydrogenchloride; diphenylphosphinopolystyrene In tetrahydrofuran for 7h; Heating;73%
With tin; acetic acid weiteres Reagens: konz. Salzsaeure;
hexamethylenetetramine
100-97-0

hexamethylenetetramine

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

C14H10O4S2*C6H12N4

C14H10O4S2*C6H12N4

Conditions
ConditionsYield
In ethanol at 20℃; for 336000h;85%
7-fluoro-1H-indole
387-44-0

7-fluoro-1H-indole

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

C15H10FNO2S

C15H10FNO2S

Conditions
ConditionsYield
With sodium hydroxide In water; isopropyl alcohol at 130℃; Green chemistry;85%
1,10-Phenanthroline
66-71-7

1,10-Phenanthroline

copper(II) choride dihydrate

copper(II) choride dihydrate

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

diaqua(1,10-phenanthroline)copper(II) sulfate

diaqua(1,10-phenanthroline)copper(II) sulfate

B

[Cu(2,2'-thiodibenzoic acid)(1,10-phenanthroline)(H2O)]2*2H2O*2DMF

[Cu(2,2'-thiodibenzoic acid)(1,10-phenanthroline)(H2O)]2*2H2O*2DMF

Conditions
ConditionsYield
With sodium hydroxide In water at 20℃; pH=7.2;A 85%
B 15%
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

sulfanilamide
63-74-1

sulfanilamide

DIBA-1
171744-39-1

DIBA-1

Conditions
ConditionsYield
With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane; N,N-dimethyl-formamide at 20℃; for 3h;83%
4-fluoroindole
387-43-9

4-fluoroindole

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

C15H10FNO2S

C15H10FNO2S

Conditions
ConditionsYield
With sodium hydroxide In water; isopropyl alcohol at 130℃; Green chemistry;83%
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

A

2,2'-dithiodibenzoic acid dichloride
19602-82-5

2,2'-dithiodibenzoic acid dichloride

B

1-(2,4,6-trichlorophenyl)-3-(2-chloro-5-tetradecanamido)-4-{[2-(2,4-di-t-amylphenoxy)-butylcarbamoyl]-phenylthio}-5-pyrazolone

1-(2,4,6-trichlorophenyl)-3-(2-chloro-5-tetradecanamido)-4-{[2-(2,4-di-t-amylphenoxy)-butylcarbamoyl]-phenylthio}-5-pyrazolone

Conditions
ConditionsYield
With thionyl chloride In n-heptaneA 80%
B n/a
gadolinium(III) nitrate hexahydrate

gadolinium(III) nitrate hexahydrate

copper(II) chloride hexahydrate

copper(II) chloride hexahydrate

2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

[Cu(II)3Gd(III)(μ3-OH)(μ3-SH)(sulfate)(water)3]n

[Cu(II)3Gd(III)(μ3-OH)(μ3-SH)(sulfate)(water)3]n

Conditions
ConditionsYield
With N(CH2CH3)3 In water High Pressure; heating mixt. of gadolinium compd., copper compd., benzoic acid deriv., deionized water and triethylamine at 170°C for 72 h; cooling to room temp. at rate of 5°C/h, isolation of crystals, washing deionized water, elem. anal.;80%
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

2-phenoxyacetic acid
122-59-8

2-phenoxyacetic acid

2-[(9-oxo-9H-thioxanthen-2-yl)oxy]-acetic acid
84434-05-9

2-[(9-oxo-9H-thioxanthen-2-yl)oxy]-acetic acid

Conditions
ConditionsYield
With sulfuric acid at 0 - 25℃; for 1h;76%
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

methyl 2-aminopropanoate monohydrochloride
13515-97-4

methyl 2-aminopropanoate monohydrochloride

2,2'-dithiodibenzoyl bis-alanine methyl ester

2,2'-dithiodibenzoyl bis-alanine methyl ester

Conditions
ConditionsYield
Stage #1: 2,2'-dithiobenzoic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 0.666667h; Reflux;
Stage #2: methyl 2-aminopropanoate monohydrochloride With triethylamine In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 48h;
76%
2,2'-dithiobenzoic acid
119-80-2

2,2'-dithiobenzoic acid

1,2-bis(2-(hydroxymethyl)phenyl)disulfane
35190-71-7

1,2-bis(2-(hydroxymethyl)phenyl)disulfane

Conditions
ConditionsYield
With borane-THF; boron trifluoride diethyl etherate In tetrahydrofuran at 20℃; for 18h;75%
With sodium bis(2-methoxyethoxy)aluminium dihydride In benzene

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