1-(4-chloro-3-hydroxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Base Information

Chemical Name:1-(4-chloro-3-hydroxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester
CAS No.:1298046-27-1
Molecular Formula:C₁₆H₂₀ClNO₄
Molecular Weight:325.792
Hs Code.:

Synonyms:1-(4-chloro-3-hydroxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

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Chemical Property of 1-(4-chloro-3-hydroxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

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Technology Process of 1-(4-chloro-3-hydroxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

There total 3 articles about 1-(4-chloro-3-hydroxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1298046-26-0
1-(3-acetoxy-4-chloro-benzoylamino)-cycloheptanecarboxylic acid methyl ester

: 1298046-27-1
1-(4-chloro-3-hydroxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 6h; Inert atmosphere;

Reference yield:

: 34113-69-4
4-chloro-3-hydroxybenzoic acid

: 1298046-27-1
1-(4-chloro-3-hydroxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3 h / Inert atmosphere; Reflux

1.2: 1 h / Inert atmosphere; Reflux

2.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / methanol / 6 h / 20 °C / Inert atmosphere

With oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In methanol; dichloromethane;

Reference yield:

: 335013-08-6
3-acetoxy-4-chlorobenzoic acid

: 1298046-27-1
1-(4-chloro-3-hydroxy-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 6 h / 20 °C / Inert atmosphere

With oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In methanol; dichloromethane;