1-(3-acetoxy-4-chloro-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Base Information

Chemical Name:1-(3-acetoxy-4-chloro-benzoylamino)-cycloheptanecarboxylic acid methyl ester
CAS No.:1298046-26-0
Molecular Formula:C₁₈H₂₂ClNO₅
Molecular Weight:367.829
Hs Code.:

Synonyms:1-(3-acetoxy-4-chloro-benzoylamino)-cycloheptanecarboxylic acid methyl ester

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Chemical Property of 1-(3-acetoxy-4-chloro-benzoylamino)-cycloheptanecarboxylic acid methyl ester

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Technology Process of 1-(3-acetoxy-4-chloro-benzoylamino)-cycloheptanecarboxylic acid methyl ester

There total 2 articles about 1-(3-acetoxy-4-chloro-benzoylamino)-cycloheptanecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 335013-08-6
3-acetoxy-4-chlorobenzoic acid

: 92398-50-0
methyl 1-amino-cycloheptanecarboxylate hydrochloride

: 1298046-26-0
1-(3-acetoxy-4-chloro-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Guidance literature:: 3-acetoxy-4-chlorobenzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; Inert atmosphere;

methyl 1-amino-cycloheptanecarboxylate hydrochloride; With sodium hydrogencarbonate; In dichloromethane; ethyl acetate; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 34113-69-4
4-chloro-3-hydroxybenzoic acid

: 1298046-26-0
1-(3-acetoxy-4-chloro-benzoylamino)-cycloheptanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3 h / Inert atmosphere; Reflux

1.2: 1 h / Inert atmosphere; Reflux

2.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;