Benzyl O-(3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:Benzyl O-(3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:121845-01-0
Molecular Formula:C₅₇H₆₂O₁₁
Molecular Weight:923.113
Hs Code.:

Synonyms:Benzyl O-(3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of Benzyl O-(3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of Benzyl O-(3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 4 articles about Benzyl O-(3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18404-73-4
(2R,3R,4R,5S,6R)-2-(benzyloxy)-5-(((3aS,4R,6S,7R,7aR)-7-hydroxy-4-(hydroxymethyl)-2,2-dimethyltetrahydro-4H-[1,3]dioxolo[4,5-c]pyran-6-yl)oxy)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4-diol

: 121845-01-0
Benzyl O-(3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / 80percent NaH / dimethylformamide / 15 h / Ambient temperature

2: 95 percent / acetic acid / H₂O / 1.5 h / 100 °C

3: 1.) dibutyltin oxide, 2.) tetrabutylammonium iodide / 1.) benzene, 15 h, reflux, 2.) benzene, 60 degC, 6 h

With tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; acetic acid; In water; N,N-dimethyl-formamide;

Reference yield:

: 59263-35-3
(3aS,4R,6S,7R,7aS)-7-(benzyloxy)-4-((benzyloxy)methyl)-2,2-dimethyl-6-(((2R,3R,4S,5R,6R)-4,5,6-tris(benzyloxy)-2-((benzyloxy)methyl)tetrahydro-2H-pyran-3-yl)oxy)tetrahydro-4H-[1,3]dioxolo[4,5-c]pyran

: 121845-01-0
Benzyl O-(3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / acetic acid / H₂O / 1.5 h / 100 °C

2: 1.) dibutyltin oxide, 2.) tetrabutylammonium iodide / 1.) benzene, 15 h, reflux, 2.) benzene, 60 degC, 6 h

With tetra-(n-butyl)ammonium iodide; di(n-butyl)tin oxide; acetic acid; In water;

Reference yield:

: 100-39-0
benzyl bromide

: 121845-01-0
Benzyl O-(3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / 80percent NaH / dimethylformamide / 15 h / Ambient temperature

2: 95 percent / acetic acid / H₂O / 1.5 h / 100 °C

3: 1.) dibutyltin oxide, 2.) tetrabutylammonium iodide / 1.) benzene, 15 h, reflux, 2.) benzene, 60 degC, 6 h

With tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; acetic acid; In water; N,N-dimethyl-formamide;