[1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate

Base Information

Chemical Name:[1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate
CAS No.:1447992-82-6
Molecular Formula:BF₄*C₂₂H₂₈N₃O
Molecular Weight:437.288
Hs Code.:

Synonyms:[1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate

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Technology Process of [1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate

There total 3 articles about [1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 13826-83-0
ammonium tetrafluroborate

: 1447992-76-8
N¹-{2-(4-morpholinyl)phenyl}-N²-(2,4,6-trimethylphenyl)-1,2-ethanediamine

: 122-51-0
orthoformic acid triethyl ester

: 1447992-82-6
[1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate

Guidance literature:: at 110 ℃; for 0.5h; Inert atmosphere;
DOI:10.1139/cjc-2013-0132

Reference yield:

: 444325-38-6
N-2,4,6-trimethylphenyl-(1,2-diaminoethane)

: 1447992-82-6
[1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; sodium t-butanolate / toluene / 2.5 h / 110 °C / Inert atmosphere; Glovebox

2: 0.5 h / 110 °C / Inert atmosphere

With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; sodium t-butanolate; In toluene;
DOI:10.1139/cjc-2013-0132

Reference yield:

: 87698-82-6
4-(2-bromophenyl)morpholine

: 1447992-82-6
[1-mesityl-3-{2-(4-morpholinyl)phenyl}imidazolidin-1-ylium] tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; sodium t-butanolate / toluene / 2.5 h / 110 °C / Inert atmosphere; Glovebox

2: 0.5 h / 110 °C / Inert atmosphere

With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; sodium t-butanolate; In toluene;
DOI:10.1139/cjc-2013-0132