C₄₁H₄₈N₂O₁₀

Base Information

Chemical Name:C₄₁H₄₈N₂O₁₀
CAS No.:943000-39-3
Molecular Formula:C₄₁H₄₈N₂O₁₀
Molecular Weight:728.84
Hs Code.:

C<sub>41</sub>H<sub>48</sub>N<sub>2</sub>O<sub>10</sub>

Synonyms:C₄₁H₄₈N₂O₁₀

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Chemical Property of C₄₁H₄₈N₂O₁₀

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Technology Process of C₄₁H₄₈N₂O₁₀

There total 11 articles about C₄₁H₄₈N₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 943000-28-0
C₂₇H₄₂O₄

: 122-04-3
4-nitro-benzoyl chloride

: 943000-39-3
C₄₁H₄₈N₂O₁₀

Guidance literature:: In pyridine; dichloromethane; at 45 ℃; for 24h;
DOI:10.1021/ja0705487

Reference yield:

: 78179-61-0
3β-acetoxy-12-keto-5α-spirostan-14-ene

: 943000-39-3
C₄₁H₄₈N₂O₁₀

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium borohydride / CH₂Cl₂; methanol / -90 - 23 °C

2.1: 10.5 g / 4-N,N-dimethylaminopyridine / CH₂Cl₂; pyridine / 4.5 h / 23 °C

3.1: 93 percent / NaCNBH₃; acetic acid / 2.5 h

4.1: tributylphosphine; 2-nitrophenyl selenocyanate; pyridine / 40 h / 23 °C

4.2: 67 percent / aq. H₂O₂ / CH₂Cl₂ / 0 - 11 °C

5.1: mercury(II) acetate / tetrahydrofuran; H₂O / 16 h / 23 °C

5.2: 88 percent / NaBH₄ / tetrahydrofuran; H₂O / 3 h

6.1: 28 percent / iodine; iodobenzene diacetate / hexane; CH₂Cl₂ / 2 h

7.1: 100 percent / potassium carbonate; methanol / tetrahydrofuran / 24 h / 40 °C

8.1: 99 percent / CH₂Cl₂; pyridine / 24 h / 45 °C

With pyridine; methanol; sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; tributylphosphine; [bis(acetoxy)iodo]benzene; mercury(II) diacetate; iodine; sodium cyanoborohydride; potassium carbonate; acetic acid; dmap; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; 4.1: Grieco reaction / 6.1: Suarez iodine(III) oxidation;
DOI:10.1021/ja0705487

Reference yield:

: 6917-04-0
(25R)-3β-Acetoxy-12,13-seco-5α-spirost-13-en-12-on

: 943000-39-3
C₄₁H₄₈N₂O₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: 1.58 g / boron trifluoride diethyl etherate / toluene / 1 h / 0 °C

2.1: Jones reagent / acetone / 0 - 23 °C

3.1: sodium borohydride / CH₂Cl₂; methanol / -90 - 23 °C

4.1: 10.5 g / 4-N,N-dimethylaminopyridine / CH₂Cl₂; pyridine / 4.5 h / 23 °C

5.1: 93 percent / NaCNBH₃; acetic acid / 2.5 h

6.1: tributylphosphine; 2-nitrophenyl selenocyanate; pyridine / 40 h / 23 °C

6.2: 67 percent / aq. H₂O₂ / CH₂Cl₂ / 0 - 11 °C

7.1: mercury(II) acetate / tetrahydrofuran; H₂O / 16 h / 23 °C

7.2: 88 percent / NaBH₄ / tetrahydrofuran; H₂O / 3 h

8.1: 28 percent / iodine; iodobenzene diacetate / hexane; CH₂Cl₂ / 2 h

9.1: 100 percent / potassium carbonate; methanol / tetrahydrofuran / 24 h / 40 °C

10.1: 99 percent / CH₂Cl₂; pyridine / 24 h / 45 °C

With pyridine; methanol; sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; jones reagent; tributylphosphine; [bis(acetoxy)iodo]benzene; mercury(II) diacetate; iodine; sodium cyanoborohydride; potassium carbonate; acetic acid; dmap; boron trifluoride diethyl etherate; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; acetone; toluene; 2.1: Jones oxidation / 6.1: Grieco reaction / 8.1: Suarez iodine(III) oxidation;
DOI:10.1021/ja0705487