2,2'-bis(benzyloxy)biphenyl-3,3'-diyldiboronic acid

Base Information

Chemical Name:2,2'-bis(benzyloxy)biphenyl-3,3'-diyldiboronic acid
CAS No.:1086433-64-8
Molecular Formula:C₂₆H₂₄B₂O₆
Molecular Weight:454.095
Hs Code.:

Synonyms:2,2'-bis(benzyloxy)biphenyl-3,3'-diyldiboronic acid

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Chemical Property of 2,2'-bis(benzyloxy)biphenyl-3,3'-diyldiboronic acid

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Technology Process of 2,2'-bis(benzyloxy)biphenyl-3,3'-diyldiboronic acid

There total 1 articles about 2,2'-bis(benzyloxy)biphenyl-3,3'-diyldiboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 1037078-35-5
2,2'-bis(benzyloxy)-3,3'-dibromobiphenyl

: 1086433-64-8
2,2'-bis(benzyloxy)biphenyl-3,3'-diyldiboronic acid

Guidance literature:: 2,2'-bis(benzyloxy)-3,3'-dibromobiphenyl; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; at -78 - 0 ℃; for 2h; Inert atmosphere;

With sodium hydroxide; water; In tetrahydrofuran; for 2h;
DOI:10.1021/ja802308a

Reference yield:

: 1086433-64-8
2,2'-bis(benzyloxy)biphenyl-3,3'-diyldiboronic acid

: 1037078-38-8
4-bromo-N₂,N₆-bis(2-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide

: 1037078-42-4
4,4'-(2,2'-bis(benzyloxy)biphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; for 24h; Reflux; Inert atmosphere;
DOI:10.1021/ja802308a

Reference yield:

: 1086433-64-8
2,2'-bis(benzyloxy)biphenyl-3,3'-diyldiboronic acid

: 1037078-37-7
4-bromo-N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide

: 1037078-41-3
4,4'-(2,2'-bis(benzyloxy)biphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; for 24h; Reflux; Inert atmosphere;
DOI:10.1021/ja802308a