(R)-2-chloro-4-(1,5,5-trimethylhydantyl)butanoic acid pentachlorophenyl ester

Base Information

Chemical Name:(R)-2-chloro-4-(1,5,5-trimethylhydantyl)butanoic acid pentachlorophenyl ester
CAS No.:860803-14-1
Molecular Formula:C₁₆H₁₄Cl₆N₂O₄
Molecular Weight:511.016
Hs Code.:

Synonyms:(R)-2-chloro-4-(1,5,5-trimethylhydantyl)butanoic acid pentachlorophenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-chloro-4-(1,5,5-trimethylhydantyl)butanoic acid pentachlorophenyl ester

Chemical Property:

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Technology Process of (R)-2-chloro-4-(1,5,5-trimethylhydantyl)butanoic acid pentachlorophenyl ester

There total 1 articles about (R)-2-chloro-4-(1,5,5-trimethylhydantyl)butanoic acid pentachlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-(1,5,5-trimethylhydantyl)butanoyl chloride

: 21306-21-8
2,2,3,4,5,6-hexachloro-cyclohexa-2,4-dien-1-one

: (S)-2-chloro-4-(1,5,5-trimethylhydantyl)butanoic acid pentachlorophenyl ester

: 860803-14-1
(R)-2-chloro-4-(1,5,5-trimethylhydantyl)butanoic acid pentachlorophenyl ester

Guidance literature:: With terephthaloylquinine Wang resin; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 ℃; for 3h; Title compound not separated from byproducts;
DOI:10.1021/ol050980y

Reference yield:

: 860803-14-1
(R)-2-chloro-4-(1,5,5-trimethylhydantyl)butanoic acid pentachlorophenyl ester

: 259188-38-0
Rebimastat

Guidance literature:: Multi-step reaction with 2 steps

1: 0.055 g / Celite 545 / tetrahydrofuran; methanol / 5 h

2: 0.055 g / Amberlite hydrogen sulfide resin / tetrahydrofuran; methanol / 10 h

With Amberlite hydrogen sulfide resin; Celite; In tetrahydrofuran; methanol;
DOI:10.1021/ol050980y