TpOs[N(Ph)(BPh₂)]Cl₂

Base Information

• Chemical Name: TpOs[N(Ph)(BPh₂)]Cl₂
• CAS No.: 330945-70-5
• Molecular Formula: C₂₇H₂₅B₂Cl₂N₇Os
• Molecular Weight: 730.27
• Mol file: 330945-70-5.mol

Synonyms:TpOs[N(Ph)(BPh₂)]Cl₂

Chemical Property of TpOs[N(Ph)(BPh₂)]Cl₂

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of TpOs[N(Ph)(BPh₂)]Cl₂

There total 1 articles about TpOs[N(Ph)(BPh₂)]Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

dichloro(hydrotris(1-pyrazolyl)borate)(nitrido)osmium(IV) + triphenylborane (960-71-4) → TpOs[N(Ph)(BPh2)]Cl2 (330945-70-5)

Guidance literature:

In benzene; a flask charged with Os-contg. compd. (0.368 mmol), BPh3 (0.446 mmol) and C6H6 was stirred for 5 min; filtering, layering the filtrate with hexanes, standing overnight; elem.anal.;

DOI:10.1021/ja0028424

Reference yield:

TpOs[N(Ph)(BPh2)]Cl2 (330945-70-5) + water (7732-18-5) → TpOs(NHPh)Cl2

Guidance literature:

With air; In neat (no solvent, solid phase); byproducts: HOBPh2; exposure to air or addn. of water une oxygen-free conditions; (1)H NMR studies;

DOI:10.1021/ja0028424

upstream raw materials:

triphenylborane