[((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile

Base Information

• Chemical Name: [((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile
• CAS No.: 710307-07-6
• Molecular Formula: C₁₈H₁₉ClN₂
• Molecular Weight: 298.815

Synonyms:[((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile

Chemical Property of [((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile

Chemical Property:

Purity/Quality:

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Technology Process of [((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile

There total 2 articles about [((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2--2-phenylethanenitrile (710307-06-5) → [((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile (710307-07-6)

Guidance literature:

With sulfuryl dichloride; In dichloromethane;

DOI:10.1016/j.tetlet.2004.03.092

Reference yield:

(2S,4S,5R)-3,4-dimethyl-2,5-diphenyloxazolidine (89675-44-5) → [((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile (710307-07-6)

Guidance literature:

Multi-step reaction with 2 steps

1: citric acid / ethanol; H₂O

2: SO₂Cl / CH₂Cl₂

With sulfuryl dichloride; citric acid; In ethanol; dichloromethane; water;

DOI:10.1016/j.tetlet.2004.03.092

Reference yield: 11.0%

[((1S,2R)-2-Chloro-1-methyl-2-phenyl-ethyl)-methyl-amino]-phenyl-acetonitrile (710307-07-6) → (5R,6S)-6,7-Dimethyl-5,8-diphenyl-5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyrazine

Guidance literature:

With sodium azide; In dimethyl sulfoxide; at 150 ℃; for 1h;

DOI:10.1016/j.tetlet.2004.03.092

upstream raw materials:

2--2-phenylethanenitrile

(2S,4S,5R)-3,4-dimethyl-2,5-diphenyloxazolidine

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