N'-(bis(3-(trifluoromethyl)phenyl)methylene)-4-methylbenzenesulfonohydrazide

Base Information

• Chemical Name: N'-(bis(3-(trifluoromethyl)phenyl)methylene)-4-methylbenzenesulfonohydrazide
• CAS No.: 1269207-60-4
• Molecular Formula: C₂₂H₁₆F₆N₂O₂S
• Molecular Weight: 486.438

Synonyms:N'-(bis(3-(trifluoromethyl)phenyl)methylene)-4-methylbenzenesulfonohydrazide

Chemical Property of N'-(bis(3-(trifluoromethyl)phenyl)methylene)-4-methylbenzenesulfonohydrazide

Chemical Property:

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Technology Process of N'-(bis(3-(trifluoromethyl)phenyl)methylene)-4-methylbenzenesulfonohydrazide

There total 1 articles about N'-(bis(3-(trifluoromethyl)phenyl)methylene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'-bis(trifluoromethyl)benzophenone (1868-00-4) + toluene-4-sulfonic acid hydrazide (1576-35-8) → N'-(bis(3-(trifluoromethyl)phenyl)methylene)-4-methylbenzenesulfonohydrazide (1269207-60-4)

Guidance literature:

In methanol; Reflux;

DOI:10.1021/ja111249p

Reference yield: 99.0%

2-ethyl-[1,2,4] triazolo[4,3-a]pyridin-2-ium tetrafluoroborate + N'-(bis(3-(trifluoromethyl)phenyl)methylene)-4-methylbenzenesulfonohydrazide (1269207-60-4) → 3-((bis(3-(trifluoromethyl)phenyl)methylene)hydrazono)-2-ethyl-2,3-dihydro-[1,2,4]triazolo[4,3-a]pyridine

Guidance literature:

With potassium tert-butylate; In N,N-dimethyl-formamide; at 80 ℃; for 2h; Schlenk technique; Inert atmosphere;

DOI:10.1002/adsc.201700241

Reference yield: 38.0%

benzoxazole (273-53-0,29791-96-6) + N'-(bis(3-(trifluoromethyl)phenyl)methylene)-4-methylbenzenesulfonohydrazide (1269207-60-4) → 2-(bis(3-(trifluoromethyl)phenyl)methyl)benzo[d]oxazole (1269207-08-0)

Guidance literature:

With copper(l) iodide; lithium tert-butoxide; In toluene; at 110 ℃; for 1.5h; Inert atmosphere;

DOI:10.1021/ja111249p

upstream raw materials:

3,3'-bis(trifluoromethyl)benzophenone

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

2-(bis(3-(trifluoromethyl)phenyl)methyl)benzo[d]oxazole

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