dimethylphenyl[(Z)-4-(tetrahydropyran-2-yloxy)but-1-enyl]silane

Base Information

• Chemical Name: dimethylphenyl[(Z)-4-(tetrahydropyran-2-yloxy)but-1-enyl]silane
• CAS No.: 122888-45-3
• Molecular Formula: C₁₇H₂₆O₂Si
• Molecular Weight: 290.478
• Mol file: 122888-45-3.mol

Synonyms:dimethylphenyl[(Z)-4-(tetrahydropyran-2-yloxy)but-1-enyl]silane

Chemical Property of dimethylphenyl[(Z)-4-(tetrahydropyran-2-yloxy)but-1-enyl]silane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of dimethylphenyl[(Z)-4-(tetrahydropyran-2-yloxy)but-1-enyl]silane

There total 1 articles about dimethylphenyl[(Z)-4-(tetrahydropyran-2-yloxy)but-1-enyl]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

dimethyl(phenyl)(4-((tetrahydro-2H-pyran-2-yl)oxy)but-1-yn-1-yl)-silane (122888-52-2) → dimethylphenyl[(Z)-4-(tetrahydropyran-2-yloxy)but-1-enyl]silane (122888-45-3)

Guidance literature:

With diisobutylaluminium hydride; In diethyl ether; hexane; at 0 - 20 ℃;

DOI:10.1016/j.tet.2008.10.108

Reference yield: 91.0%

dimethylphenyl[(Z)-4-(tetrahydropyran-2-yloxy)but-1-enyl]silane (122888-45-3) → (Z)-4-(dimethyl(phenyl)silyl)but-3-en-1-ol (122888-53-3)

Guidance literature:

With water; toluene-4-sulfonic acid; In methanol; at 20 ℃; for 3h;

DOI:10.1016/j.tet.2008.10.108

upstream raw materials:

dimethyl(phenyl)(4-((tetrahydro-2H-pyran-2-yl)oxy)but-1-yn-1-yl)-silane

Downstream raw materials:

(Z)-4-(dimethyl(phenyl)silyl)but-3-en-1-ol