N-(2-butyl-3-(4-(3-(dibutylamino)propoxy)benzoyl)benzofuran-5-yl)acetamide

Base Information

• Chemical Name: N-(2-butyl-3-(4-(3-(dibutylamino)propoxy)benzoyl)benzofuran-5-yl)acetamide
• CAS No.: 1278585-69-5
• Molecular Formula: C₃₂H₄₄N₂O₄
• Molecular Weight: 520.712

Synonyms:N-(2-butyl-3-(4-(3-(dibutylamino)propoxy)benzoyl)benzofuran-5-yl)acetamide

Chemical Property of N-(2-butyl-3-(4-(3-(dibutylamino)propoxy)benzoyl)benzofuran-5-yl)acetamide

Chemical Property:

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Technology Process of N-(2-butyl-3-(4-(3-(dibutylamino)propoxy)benzoyl)benzofuran-5-yl)acetamide

There total 19 articles about N-(2-butyl-3-(4-(3-(dibutylamino)propoxy)benzoyl)benzofuran-5-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.6%

2-n-butyl-3-(4-(3-chloropropoxy)benzoyl)-5-acetamidobenzofuran + dibutylamine (111-92-2) → N-(2-butyl-3-(4-(3-(dibutylamino)propoxy)benzoyl)benzofuran-5-yl)acetamide (1278585-69-5)

Guidance literature:

With potassium carbonate; In acetonitrile; for 48h; Reflux;

Reference yield: 74.9%

4-(3-di-n-butylaminopropoxy)benzoyl chloride (478158-85-9) + (2-n-butyl-benzofuran-5-yl)-acetamide (526196-92-9) → N-(2-butyl-3-(4-(3-(dibutylamino)propoxy)benzoyl)benzofuran-5-yl)acetamide (1278585-69-5)

Guidance literature:

With aluminum (III) chloride; In dichloromethane; at 2 - 20 ℃; for 5h;

Reference yield:

dibutyl-(3-chloro-propyl)-amine (36421-15-5) + 2-n-butyl-3-(4-hydroxybenzoyl)-5-acetamidobenzofuran (1278585-66-2) → N-(2-butyl-3-(4-(3-(dibutylamino)propoxy)benzoyl)benzofuran-5-yl)acetamide (1278585-69-5)

Guidance literature:

With potassium carbonate; In butanone; at 80 ℃; for 13h; Reflux;

upstream raw materials:

dibutyl-(3-chloro-propyl)-amine

2-n-butyl-3-(4-hydroxybenzoyl)-5-acetamidobenzofuran

4-acetaminophenol

methyl α-bromo heptanoate

Downstream raw materials:

2-n-butyl-3-{4-[3-(di-n-butylamino)propoxy]benzoyl}-5-aminobenzofuran hydrochloride

5-amino-2-n-butyl-3-[4-(3-di-n-butylamino propoxy)benzoyl]benzofuran bisoxalate

(5-amino-2-butyl-benzofuran-3-yl)-[4-(3-dibutylamino-propoxy)-phenyl]-methanone

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