cis-bis(4-hydroxycyclohexylamine)diiodoplatinum(II)

Base Information

Chemical Name:cis-bis(4-hydroxycyclohexylamine)diiodoplatinum(II)
CAS No.:127225-15-4
Molecular Formula:C₁₂H₂₆I₂N₂O₂Pt
Molecular Weight:679.24
Hs Code.:

Synonyms:cis-bis(4-hydroxycyclohexylamine)diiodoplatinum(II)

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Chemical Property of cis-bis(4-hydroxycyclohexylamine)diiodoplatinum(II)

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Technology Process of cis-bis(4-hydroxycyclohexylamine)diiodoplatinum(II)

There total 1 articles about cis-bis(4-hydroxycyclohexylamine)diiodoplatinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10025-99-7
potassium tetrachloroplatinate(II)

: 6850-65-3
p-hydroxycyclohexylamine

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 127225-15-4
cis-bis(4-hydroxycyclohexylamine)diiodoplatinum(II)

Guidance literature:: In water; A concd. soln. of KI is added to a soln. of K2PtCl4, mixt. is stirred for 20 min, soln. is filtered with stirring into a dilute aq. soln. of the ligand.; Pptn., if the ppt. contained a trace of brown, stirring for 30-40 min, yellow ppt. is filtered off, washed with water, ethanol and ether, and dried in vac., recrystn. from DMF/water at room temp.;
DOI:10.1039/DT9900000307

Reference yield: 85.0%

: 127225-15-4
cis-bis(4-hydroxycyclohexylamine)diiodoplatinum(II)

: cis-bis(4-hydroxycyclohexylamine)dinitratoplatinum(II)*1.8H₂O

Guidance literature:: With silver nitrate; In acetone; byproducts: AgI; To a soln. of Pt-compd. powdered AgNO3 is added, stirring for 5-20 min,; Soln. is filtered through cellulose and evapd., dissolving in acetone, refiltered , addn. of toluene or ether, cooling to 5°C for several hours, ppt. is filtered off, washed with ether, dried using a vac. pump, elem. anal.;
DOI:10.1039/DT9900000307