2-(bis((5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl)methylthio)methylene)malononitrile

Base Information

Chemical Name:2-(bis((5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl)methylthio)methylene)malononitrile
CAS No.:1293956-48-5
Molecular Formula:C₂₂H₁₂Cl₂N₆O₂S₂
Molecular Weight:527.414
Hs Code.:

Synonyms:2-(bis((5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl)methylthio)methylene)malononitrile

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Chemical Property of 2-(bis((5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl)methylthio)methylene)malononitrile

Chemical Property:

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Technology Process of 2-(bis((5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl)methylthio)methylene)malononitrile

There total 2 articles about 2-(bis((5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl)methylthio)methylene)malononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 24068-15-3
2‐(chloromethyl)‐5‐(4‐chlorophenyl)‐1,3,4‐oxadiazole

: 75-15-0,12122-00-8
carbon disulfide

: 109-77-3
malononitrile

: 1293956-48-5
2-(bis((5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl)methylthio)methylene)malononitrile

Guidance literature:: carbon disulfide; malononitrile; With sodium ethanolate; at 0 ℃; for 1h;

2‐(chloromethyl)‐5‐(4‐chlorophenyl)‐1,3,4‐oxadiazole; In ethanol; at 20 - 30 ℃;
DOI:10.1016/j.ejmech.2011.01.063

Reference yield:

: 536-40-3
4-chlorobenzoic acid hydrazide

: 1293956-48-5
2-(bis((5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl)methylthio)methylene)malononitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / Reflux

2.1: sodium ethanolate / 1 h / 0 °C

2.2: 20 - 30 °C

With sodium ethanolate; trichlorophosphate;
DOI:10.1016/j.ejmech.2011.01.063