diethyl 1-(4-bromophenyl)ethenylphosphonate

Base Information

Chemical Name:diethyl 1-(4-bromophenyl)ethenylphosphonate
CAS No.:1159205-36-3
Molecular Formula:C₁₂H₁₆BrO₃P
Molecular Weight:319.135
Hs Code.:

Synonyms:diethyl 1-(4-bromophenyl)ethenylphosphonate

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Chemical Property of diethyl 1-(4-bromophenyl)ethenylphosphonate

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Technology Process of diethyl 1-(4-bromophenyl)ethenylphosphonate

There total 7 articles about diethyl 1-(4-bromophenyl)ethenylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 38318-52-4
α-bromovinylphosphonic acid diethyl ester

: 374564-35-9
potassium 4-bromophenyltrifluoroborate

: 1159205-36-3
diethyl 1-(4-bromophenyl)ethenylphosphonate

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; In water; toluene; at 20 - 90 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1039/c7ob02267k

Reference yield: 92.0%

: 5467-74-3
4-Bromophenylboronic acid

: 243137-79-3
1,1,2,2,3,3,4,4,4-nonafluoro-butane-1-sulfonic acid 1-(diethoxy-phosphoryl)-vinyl ester

: 1159205-36-3
diethyl 1-(4-bromophenyl)ethenylphosphonate

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate; In toluene; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/cjoc.201500414