methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside
CAS No.:1388150-08-0
Molecular Formula:C₂₈H₃₉NO₁₅
Molecular Weight:629.615
Hs Code.:

methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

Synonyms:methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

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Chemical Property of methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

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Technology Process of methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

There total 4 articles about methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1388150-07-9
methyl (2-O-acetyl-3-O-methyl-α-L-idopyranosyl)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

: 74-88-4
methyl iodide

: 1388150-08-0
methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

Guidance literature:: methyl (2-O-acetyl-3-O-methyl-α-L-idopyranosyl)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside; With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water; sodium hydrogencarbonate; In tetrahydrofuran; at 0 - 20 ℃; for 4.5h; Inert atmosphere;

methyl iodide; With potassium hydrogencarbonate; In N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;

Reference yield:

: 1388150-05-7
methyl (4,6-O-isopropylidene-3-O-methyl-α-L-idopyranosyl)-(1->4)-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

: 1388150-08-0
methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; triethylamine / dichloromethane / 2.17 h / 0 - 20 °C

2.1: acetic acid / 16 h / 20 °C

3.1: sodium hydrogencarbonate; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / tetrahydrofuran / 4.5 h / 0 - 20 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

With dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water; sodium hydrogencarbonate; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1388150-06-8
methyl (2-O-acetyl-4,6-O-isopropylidene-3-O-methyl-α-L-idopyranosyl)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

: 1388150-08-0
methyl (methyl 2-O-acetyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-[(benzyloxy)carbonyl]amino-2-deoxy-3-O-methyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / 16 h / 20 °C

2.1: sodium hydrogencarbonate; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / tetrahydrofuran / 4.5 h / 0 - 20 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran;