Benzyloxycarbonylamino-acetic acid 3-ethylcarbamoyl-2-hydroxy-phenyl ester

Base Information

• Chemical Name: Benzyloxycarbonylamino-acetic acid 3-ethylcarbamoyl-2-hydroxy-phenyl ester
• CAS No.: 16859-24-8
• Molecular Formula: C₁₉H₂₀N₂O₆
• Molecular Weight: 372.378

Synonyms:Benzyloxycarbonylamino-acetic acid 3-ethylcarbamoyl-2-hydroxy-phenyl ester

Chemical Property of Benzyloxycarbonylamino-acetic acid 3-ethylcarbamoyl-2-hydroxy-phenyl ester

Chemical Property:

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Technology Process of Benzyloxycarbonylamino-acetic acid 3-ethylcarbamoyl-2-hydroxy-phenyl ester

There total 1 articles about Benzyloxycarbonylamino-acetic acid 3-ethylcarbamoyl-2-hydroxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-ethyl-7-hydroxy-benzo[d]isoxazolium; tetrafluoroborate (16859-20-4) + N-(Benzyloxycarbonyl)glycine (1138-80-3) → Benzyloxycarbonylamino-acetic acid 3-ethylcarbamoyl-2-hydroxy-phenyl ester (16859-24-8)

Guidance literature:

Multistep reaction; (i) aq. NaOH, AcOEt, Py, (ii) /BRN= 4171999/, aq. HCl;

DOI:10.1016/S0040-4020(01)97372-7

Reference yield:

L-isoleucine (73-32-5,959215-79-3,18875-42-8) + Benzyloxycarbonylamino-acetic acid 3-ethylcarbamoyl-2-hydroxy-phenyl ester (16859-24-8) → ((benzyloxy)carbonyl)glycyl-L-isoleucine (20807-11-8)

Guidance literature:

Multistep reaction; (i) OH, (ii) /BRN= 3040634/, N,N,N',N'-tetramethyl-guanidine, DMSO;

DOI:10.1016/S0040-4020(01)97372-7

Reference yield:

L-methionine (63-68-3,26062-47-5,58576-49-1) + Benzyloxycarbonylamino-acetic acid 3-ethylcarbamoyl-2-hydroxy-phenyl ester (16859-24-8) → N-(N-benzyloxycarbonyl-glycyl)-L-methionine (3561-48-6)

Guidance literature:

Multistep reaction; (i) OH, (ii) /BRN= 3040634/, N,N,N',N'-tetramethyl-guanidine, DMSO;

DOI:10.1016/S0040-4020(01)97372-7

upstream raw materials:

2-ethyl-7-hydroxy-benzo[d]isoxazolium; tetrafluoroborate

N-(Benzyloxycarbonyl)glycine

Downstream raw materials:

(S)-2-(2-Benzyloxycarbonylamino-acetylamino)-propionic acid

(S)-2-(2-Benzyloxycarbonylamino-acetylamino)-4-methyl-pentanoic acid

((benzyloxy)carbonyl)glycyl-L-isoleucine

N-(N-benzyloxycarbonyl-glycyl)-L-methionine

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