N-(tert-butyloxycarbonyl)-L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester

Base Information

Chemical Name:N-(tert-butyloxycarbonyl)-L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester
CAS No.:1293992-21-8
Molecular Formula:C₂₉H₂₉NO₈
Molecular Weight:519.551
Hs Code.:

Synonyms:N-(tert-butyloxycarbonyl)-L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester

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Chemical Property of N-(tert-butyloxycarbonyl)-L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester

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Technology Process of N-(tert-butyloxycarbonyl)-L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester

There total 1 articles about N-(tert-butyloxycarbonyl)-L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 861820-84-0
1-chloromethyl-9-methoxy-3-oxo-3H-naphtho[2,1-b]pyran

: 3978-80-1
Boc-Tyr-OH

: 1293992-21-8
N-(tert-butyloxycarbonyl)-L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester

Guidance literature:: With potassium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.1016/j.tet.2011.01.090

Reference yield: 76.0%

: 1293992-21-8
N-(tert-butyloxycarbonyl)-L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester

: 1293992-24-1
L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2011.01.090

Reference yield:

: 1293992-21-8
N-(tert-butyloxycarbonyl)-L-tyrosine (9-methoxy-(5,6)-benzocoumarin-1-yl)methyl ester

: 60-18-4,18875-48-4,25619-78-7,30704-25-7
L-tyrosine

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

2: acetonitrile / 2.6 h / pH 7.2 / Photolysis; HEPES buffer

With trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2011.01.090