1,2-Bis<2-nitro-4-(1-carbomethoxy-2-methyl-2-propyl)-5-fluorophenoxy>ethane

Base Information

Chemical Name:1,2-Bis<2-nitro-4-(1-carbomethoxy-2-methyl-2-propyl)-5-fluorophenoxy>ethane
CAS No.:143915-24-6
Molecular Formula:C₂₆H₃₀F₂N₂O₁₀
Molecular Weight:568.528
Hs Code.:

Synonyms:1,2-Bis<2-nitro-4-(1-carbomethoxy-2-methyl-2-propyl)-5-fluorophenoxy>ethane

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Chemical Property of 1,2-Bis<2-nitro-4-(1-carbomethoxy-2-methyl-2-propyl)-5-fluorophenoxy>ethane

Chemical Property:

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Technology Process of 1,2-Bis<2-nitro-4-(1-carbomethoxy-2-methyl-2-propyl)-5-fluorophenoxy>ethane

There total 11 articles about 1,2-Bis<2-nitro-4-(1-carbomethoxy-2-methyl-2-propyl)-5-fluorophenoxy>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 143915-23-5
1,2-Bis<3-fluoro-4-(1-carbomethoxy-2-methyl-2-propyl)phenoxy>ethane

: 143915-24-6
1,2-Bis<2-nitro-4-(1-carbomethoxy-2-methyl-2-propyl)-5-fluorophenoxy>ethane

Guidance literature:: With nitric acid; acetic anhydride; In dichloromethane; at -15 ℃; for 0.333333h;
DOI:10.1002/mrc.1260300807

Reference yield:

: 372-20-3
3-fluorophenol

: 143915-24-6
1,2-Bis<2-nitro-4-(1-carbomethoxy-2-methyl-2-propyl)-5-fluorophenoxy>ethane

Guidance literature:: Multi-step reaction with 11 steps

1: 1) NaH / 1) DMF, 2) DMF, 65 deg C, 3 h

2: 93.7 percent / H₂ / 10percent Pd/C / ethanol / 24 h / 55 °C / 2280 Torr

3: 75 percent / pyridine / 2 h / 0 °C

4: 98 percent / dimethylformamide / 3 h / 60 °C

5: 53 percent / AlCl₃ / CS₂ / Heating

6: 78 percent / HOAc, NH₄OAc / benzene / 48 h / Heating

7: 43 percent / CuCl / tetrahydrofuran; diethyl ether / Ambient temperature

8: KOH, H₂O / ethane-1,2-diol / 36 h / Heating

9: 6 h / 180 °C

10: diethyl ether

11: 65 percent / HNO₃, Ac₂O / CH₂Cl₂ / 0.33 h / -15 °C

With pyridine; potassium hydroxide; aluminium trichloride; ammonium acetate; water; hydrogen; nitric acid; acetic anhydride; sodium hydride; acetic acid; copper(l) chloride; palladium on activated charcoal; In tetrahydrofuran; carbon disulfide; diethyl ether; ethanol; dichloromethane; ethylene glycol; N,N-dimethyl-formamide; benzene;
DOI:10.1002/mrc.1260300807

Reference yield:

: 143915-16-6
1-(3-Fluorophenoxy)-2-benzyloxyethane

: 143915-24-6
1,2-Bis<2-nitro-4-(1-carbomethoxy-2-methyl-2-propyl)-5-fluorophenoxy>ethane

Guidance literature:: Multi-step reaction with 10 steps

1: 93.7 percent / H₂ / 10percent Pd/C / ethanol / 24 h / 55 °C / 2280 Torr

2: 75 percent / pyridine / 2 h / 0 °C

3: 98 percent / dimethylformamide / 3 h / 60 °C

4: 53 percent / AlCl₃ / CS₂ / Heating

5: 78 percent / HOAc, NH₄OAc / benzene / 48 h / Heating

6: 43 percent / CuCl / tetrahydrofuran; diethyl ether / Ambient temperature

7: KOH, H₂O / ethane-1,2-diol / 36 h / Heating

8: 6 h / 180 °C

9: diethyl ether

10: 65 percent / HNO₃, Ac₂O / CH₂Cl₂ / 0.33 h / -15 °C

With pyridine; potassium hydroxide; aluminium trichloride; ammonium acetate; water; hydrogen; nitric acid; acetic anhydride; acetic acid; copper(l) chloride; palladium on activated charcoal; In tetrahydrofuran; carbon disulfide; diethyl ether; ethanol; dichloromethane; ethylene glycol; N,N-dimethyl-formamide; benzene;
DOI:10.1002/mrc.1260300807