methyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-β-D-arabinofuranosyl-(1→3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

Base Information

Chemical Name:methyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-β-D-arabinofuranosyl-(1→3)-2,5-di-O-benzoyl-α-D-arabinofuranoside
CAS No.:1448225-51-1
Molecular Formula:C₄₅H₄₃NO₁₂
Molecular Weight:789.836
Hs Code.:

Synonyms:methyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-β-D-arabinofuranosyl-(1→3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

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Chemical Property of methyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-β-D-arabinofuranosyl-(1→3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

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Technology Process of methyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-β-D-arabinofuranosyl-(1→3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

There total 11 articles about methyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-β-D-arabinofuranosyl-(1→3)-2,5-di-O-benzoyl-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1448225-43-1
ethyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-1-thio-α-D-arabinofuranoside

: methyl 2,5-di-O-benzoyl-α-D-arabinofuranoside

: 1448225-51-1
methyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-β-D-arabinofuranosyl-(1→3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

: 1448225-84-0
C₄₅H₄₃NO₁₂

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In 1,2-dichloro-ethane; at -30 - 30 ℃; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol401755e

Reference yield: 70.0%

: 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-α/β-D-arabinofuranosyl trichloroacetimidate

: methyl 2,5-di-O-benzoyl-α-D-arabinofuranoside

: 1448225-51-1
methyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-β-D-arabinofuranosyl-(1→3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

: 1448225-84-0
C₄₅H₄₃NO₁₂

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - 30 ℃; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol401755e

Reference yield: 56.0%

: 1448225-39-5
phenyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-1-thio-α-D-arabinofuranoside

: methyl 2,5-di-O-benzoyl-α-D-arabinofuranoside

: 1448225-51-1
methyl 2,3-di-O-benzyl-5-O-(2-pyridinecarbonyl)-β-D-arabinofuranosyl-(1→3)-2,5-di-O-benzoyl-α-D-arabinofuranoside

: 1448225-84-0
C₄₅H₄₃NO₁₂

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In 1,2-dichloro-ethane; at -30 - 42 ℃; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol401755e