N-((Z)-1-{[(tert-butyl)dimethylsilyl]oxy}prop-1-enyl)-4-methyl-N-prop-2-enylbenzamide

Base Information

Chemical Name:N-((Z)-1-{[(tert-butyl)dimethylsilyl]oxy}prop-1-enyl)-4-methyl-N-prop-2-enylbenzamide
CAS No.:319483-26-6
Molecular Formula:C₂₀H₃₁NO₂Si
Molecular Weight:345.557
Hs Code.:

Synonyms:N-((Z)-1-{[(tert-butyl)dimethylsilyl]oxy}prop-1-enyl)-4-methyl-N-prop-2-enylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((Z)-1-{[(tert-butyl)dimethylsilyl]oxy}prop-1-enyl)-4-methyl-N-prop-2-enylbenzamide

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Technology Process of N-((Z)-1-{[(tert-butyl)dimethylsilyl]oxy}prop-1-enyl)-4-methyl-N-prop-2-enylbenzamide

There total 2 articles about N-((Z)-1-{[(tert-butyl)dimethylsilyl]oxy}prop-1-enyl)-4-methyl-N-prop-2-enylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 255395-91-6
4-methyl-N-propanoyl-N-prop-2-enylbenzamide

: 319483-26-6
N-((Z)-1-{[(tert-butyl)dimethylsilyl]oxy}prop-1-enyl)-4-methyl-N-prop-2-enylbenzamide

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane; In tetrahydrofuran; at -85 ℃; for 0.75h;
DOI:10.1002/1522-2675(20001004)83:10<2712::AID-HLCA2712>3.0.CO;2-D

Reference yield:

: 88229-22-5
4-methyl-N-prop-2-enylbenzamide

: 319483-26-6
N-((Z)-1-{[(tert-butyl)dimethylsilyl]oxy}prop-1-enyl)-4-methyl-N-prop-2-enylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / Me₃SiNHCOOEt / CH₂Cl₂ / 14 h / 40 °C

2: 93 percent / LHMDS; HMPA / tetrahydrofuran / 0.75 h / -85 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; ethyl N-trimethylsilylcarbamate; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; 1: Acylation / 2: enoletherification;
DOI:10.1002/1522-2675(20001004)83:10<2712::AID-HLCA2712>3.0.CO;2-D