N^α-(9H-fluoren-9-ylmethoxycarbonyl)-N^β,N^β-bis[3-(benzyloxycarbonylamino)propyl]-L-2,3-diaminopropionic acid

Base Information

• Chemical Name: N^α-(9H-fluoren-9-ylmethoxycarbonyl)-N^β,N^β-bis[3-(benzyloxycarbonylamino)propyl]-L-2,3-diaminopropionic acid
• CAS No.: 1429403-89-3
• Molecular Formula: C₄₀H₄₄N₄O₈
• Molecular Weight: 708.811

Synonyms:N^α-(9H-fluoren-9-ylmethoxycarbonyl)-N^β,N^β-bis[3-(benzyloxycarbonylamino)propyl]-L-2,3-diaminopropionic acid

Chemical Property of N^α-(9H-fluoren-9-ylmethoxycarbonyl)-N^β,N^β-bis[3-(benzyloxycarbonylamino)propyl]-L-2,3-diaminopropionic acid

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Technology Process of N^α-(9H-fluoren-9-ylmethoxycarbonyl)-N^β,N^β-bis[3-(benzyloxycarbonylamino)propyl]-L-2,3-diaminopropionic acid

There total 1 articles about N^α-(9H-fluoren-9-ylmethoxycarbonyl)-N^β,N^β-bis[3-(benzyloxycarbonylamino)propyl]-L-2,3-diaminopropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3-[(benzyloxycarbonyl)amino]propanal (65564-05-8) + 3-amino-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine (181954-34-7) → Nα-(9H-fluoren-9-ylmethoxycarbonyl)-Nβ,Nβ-bis[3-(benzyloxycarbonylamino)propyl]-L-2,3-diaminopropionic acid (1429403-89-3)

Guidance literature:

3-[(benzyloxycarbonyl)amino]propanal; 3-amino-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; With acetic acid; In methanol; at 20 ℃; for 1h;

With sodium cyanoborohydride; In methanol; at 20 ℃;

DOI:10.1007/s00726-012-1336-5

upstream raw materials:

3-[(benzyloxycarbonyl)amino]propanal

3-amino-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

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