(4aS,9aR)-4,4a,9,9a-tetrahydro-Indeno[2,1-b]-1,4-oxazin-3(2H)-one

Base Information

Chemical Name:(4aS,9aR)-4,4a,9,9a-tetrahydro-Indeno[2,1-b]-1,4-oxazin-3(2H)-one
CAS No.:913718-34-0
Molecular Formula:C₁₁H₁₁NO₂
Molecular Weight:189.214
Hs Code.:
Mol file:913718-34-0.mol

Synonyms:(4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-one

Suppliers and Price of (4aS,9aR)-4,4a,9,9a-tetrahydro-Indeno[2,1-b]-1,4-oxazin-3(2H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Ambeed
(4aS,9aR)-4,4a,9,9a-tetrahydro-indeno[2,1-b]-1,4-oxazin-3(2H)-one 98%
5g
$ 384.00

Ambeed
(4aS,9aR)-4,4a,9,9a-tetrahydro-indeno[2,1-b]-1,4-oxazin-3(2H)-one 98%
1g
$ 128.00

Ambeed
(4aS,9aR)-4,4a,9,9a-tetrahydro-indeno[2,1-b]-1,4-oxazin-3(2H)-one 98%
250mg
$ 58.00

Ambeed
(4aS,9aR)-4,4a,9,9a-tetrahydro-indeno[2,1-b]-1,4-oxazin-3(2H)-one 98%
100mg
$ 29.00

Total 7 raw suppliers

Chemical Property of (4aS,9aR)-4,4a,9,9a-tetrahydro-Indeno[2,1-b]-1,4-oxazin-3(2H)-one

Chemical Property:

Boiling Point:433.2±45.0 °C(Predicted)
PKA:13?+-.0.20(Predicted)
Density:1.228±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

(4aS,9aR)-4,4a,9,9a-tetrahydro-indeno[2,1-b]-1,4-oxazin-3(2H)-one 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4aS,9aR)-4,4a,9,9a-tetrahydro-Indeno[2,1-b]-1,4-oxazin-3(2H)-one

There total 2 articles about (4aS,9aR)-4,4a,9,9a-tetrahydro-Indeno[2,1-b]-1,4-oxazin-3(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 7480-35-5,13286-59-4,74165-73-4,126456-43-7,136030-00-7,140632-19-5,140632-20-8
(1S,2R)-1-amino-2-indanol

: 105-39-5
chloroacetic acid ethyl ester

: 913718-34-0
(4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-one

Guidance literature:: (1S,2R)-1-amino-2-indanol; With sodium tetrahydroborate; In tetrahydrofuran; at 0 - 70 ℃;

chloroacetic acid ethyl ester; In tetrahydrofuran; at 0 ℃; for 2.5h; Reflux;
DOI:10.1016/j.tetasy.2011.04.001

Reference yield: 49.0%

: 913718-34-0
(4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-one

Guidance literature:

Reference yield: 60.0%

: 913718-34-0
(4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-one

: 122-51-0
orthoformic acid triethyl ester

: 84828-07-9
2,6-diethylphenylhydrazine

: (5aR,10bS)-2-(2,6-diethylphenyl)-4,5a,6,10b-tetrahydroindeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazin-2-ium tetrafluoroborate

Guidance literature:: (4aS,9aR)-4,4a,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-3(2H)-one; With trimethoxonium tetrafluoroborate;

2,6-diethylphenylhydrazine; In dichloromethane; at 20 ℃;

orthoformic acid triethyl ester; In chlorobenzene; at 110 ℃;
DOI:10.1021/ja910666n