(6E,10E,14E,18E,22E,26E)-28-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol

Base Information

• Chemical Name: (6E,10E,14E,18E,22E,26E)-28-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol
• CAS No.: 66958-30-3
• Molecular Formula: C₅₈H₈₀O₅
• Molecular Weight: 857.27

Synonyms:(6E,10E,14E,18E,22E,26E)-28-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol

Chemical Property of (6E,10E,14E,18E,22E,26E)-28-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of (6E,10E,14E,18E,22E,26E)-28-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol

There total 4 articles about (6E,10E,14E,18E,22E,26E)-28-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-[(3E,7E,11E,15E,19E,23E)-25-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane (66958-27-8) → (6E,10E,14E,18E,22E,26E)-28-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol (66958-30-3)

Guidance literature:

With lithium diisopropyl amide;

Reference yield:

Acetic acid (4E,8E,12E,16E,20E,24E)-26-(2,5-bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-1-isopropenyl-4,8,12,16,20,24-hexamethyl-hexacosa-4,8,12,16,20,24-hexaenyl ester (66958-29-0) → (6E,10E,14E,18E,22E,26E)-28-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol (66958-30-3)

Guidance literature:

With sodium hydroxide;

Reference yield:

Acetic acid (4E,8E,12E,16E,20E,24E)-26-(2,5-bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-1-(1-hydroxy-1-methyl-ethyl)-4,8,12,16,20,24-hexamethyl-hexacosa-4,8,12,16,20,24-hexaenyl ester (66958-28-9) → (6E,10E,14E,18E,22E,26E)-28-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol (66958-30-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) SOCl₂, (ii) Py

2: aq. NaOH

With sodium hydroxide;

upstream raw materials:

3-[(3E,7E,11E,15E,19E,23E)-25-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane

Acetic acid (4E,8E,12E,16E,20E,24E)-26-(2,5-bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-1-isopropenyl-4,8,12,16,20,24-hexamethyl-hexacosa-4,8,12,16,20,24-hexaenyl ester

Acetic acid (4E,8E,12E,16E,20E,24E)-26-(2,5-bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-1-(1-hydroxy-1-methyl-ethyl)-4,8,12,16,20,24-hexamethyl-hexacosa-4,8,12,16,20,24-hexaenyl ester

Downstream raw materials:

ubiquinone-45

ubiquinone 8

1,4-Bis-benzyloxy-2,3-dimethoxy-5-methyl-6-[(2E,6E,10E,14E,18E,22E,26E)-3,7,11,15,19,23,27,31-octamethyl-29-(toluene-4-sulfonyl)-dotriaconta-2,6,10,14,18,22,26,30-octaenyl]-benzene

1,4-Bis-benzyloxy-2,3-dimethoxy-5-methyl-6-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethyl-29-(toluene-4-sulfonyl)-hexatriaconta-2,6,10,14,18,22,26,30,34-nonaenyl]-benzene

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