(E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Base Information

Chemical Name:(E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester
CAS No.:137585-76-3
Molecular Formula:C₂₃H₂₄O₅
Molecular Weight:380.441
Hs Code.:

Synonyms:(E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Suppliers and Price of (E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

There total 1 articles about (E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 18439-39-9
2,2-dimethyl-5-phenylmethyl-(3aR,5R,6aR)-perhydrofuro[2,3-d][1,3]-dioxol-(6S)-ol

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 137585-76-3
(E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0957-4166(00)82200-4

Reference yield:

: 1826-67-1
vinyl magnesium bromide

: 137585-76-3
(E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

: 137585-80-9,137586-12-0
3-Phenyl-pent-4-enoic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Guidance literature:: With copper(I) bromide dimethylsulfide complex; Yield given. Multistep reaction; 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 2 h;
DOI:10.1016/S0957-4166(00)82200-4

Reference yield:

: 137585-76-3
(E)-3-Phenyl-acrylic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

: 1730-25-2
allylmagnesium bromide

: 137585-85-4,137586-13-1
3-Phenyl-hex-5-enoic acid (3aR,5R,6S,6aR)-5-benzyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Guidance literature:: With copper(I) bromide dimethylsulfide complex; Yield given. Multistep reaction; 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 2 h;
DOI:10.1016/S0957-4166(00)82200-4