4-hydroxy-5,6-dimethyl-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-pyridinecarboxylic acid

Base Information

Chemical Name:4-hydroxy-5,6-dimethyl-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-pyridinecarboxylic acid
CAS No.:1213565-66-2
Molecular Formula:C₁₅H₁₅NO₄
Molecular Weight:273.288
Hs Code.:

Synonyms:4-hydroxy-5,6-dimethyl-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-pyridinecarboxylic acid

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Chemical Property of 4-hydroxy-5,6-dimethyl-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-pyridinecarboxylic acid

Chemical Property:

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Technology Process of 4-hydroxy-5,6-dimethyl-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-pyridinecarboxylic acid

There total 1 articles about 4-hydroxy-5,6-dimethyl-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-pyridinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 686266-59-1
3-benzyl-4,5-dimethyl-2H-1,3-oxazine-2,6(3H)-dione

: 105-53-3
diethyl malonate

: 1213565-66-2
4-hydroxy-5,6-dimethyl-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-pyridinecarboxylic acid

Guidance literature:: 3-benzyl-4,5-dimethyl-2H-1,3-oxazine-2,6(3H)-dione; diethyl malonate; With sodium hydride; In tetrahydrofuran; for 2.5h; Reflux;

With hydrogenchloride; In tetrahydrofuran; water;

Reference yield:

: 1213565-66-2
4-hydroxy-5,6-dimethyl-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-pyridinecarboxylic acid

: 623-33-6
glycine ethyl ester hydrochloride

: C₁₉H₂₂N₂O₅

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 20h;