Technology Process of C62H82O6S2
There total 10 articles about C62H82O6S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hexamethyldisilazane;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at -20 - 0 ℃;
for 0.5h;
Inert atmosphere;
Cooling with acetone-dry ice;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: phosphorus tribromide / tetrahydrofuran / 3 h / 0 °C
2.1: potassium tert-butylate / tetrahydrofuran; N,N-dimethyl-formamide / 2.67 h / -78 °C
2.2: -78 - 20 °C
3.1: sodium hydroxide; water / methanol / 1 h / 20 °C / pH 12
4.1: phosphorus tribromide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Cooling with acetone-dry ice
5.1: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 0.5 h / -20 - 0 °C / Inert atmosphere; Cooling with acetone-dry ice
With
potassium tert-butylate; water; sodium hexamethyldisilazane; phosphorus tribromide; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium tert-butylate / tetrahydrofuran; N,N-dimethyl-formamide / 2.67 h / -78 °C
1.2: -78 - 20 °C
2.1: sodium hydroxide; water / methanol / 1 h / 20 °C / pH 12
3.1: phosphorus tribromide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Cooling with acetone-dry ice
4.1: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 0.5 h / -20 - 0 °C / Inert atmosphere; Cooling with acetone-dry ice
With
potassium tert-butylate; water; sodium hexamethyldisilazane; phosphorus tribromide; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;