phenylsulfonyl hexaprenyl bromide

Base Information

Chemical Name:phenylsulfonyl hexaprenyl bromide
CAS No.:1597486-86-6
Molecular Formula:C₃₆H₅₃BrO₂S
Molecular Weight:629.786
Hs Code.:

Synonyms:phenylsulfonyl hexaprenyl bromide

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Chemical Property of phenylsulfonyl hexaprenyl bromide

Chemical Property:

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Technology Process of phenylsulfonyl hexaprenyl bromide

There total 8 articles about phenylsulfonyl hexaprenyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-28-5
Farnesol

: 1597486-86-6
phenylsulfonyl hexaprenyl bromide

Guidance literature:: Multi-step reaction with 4 steps

1.1: phosphorus tribromide / tetrahydrofuran / 3 h / 0 °C

2.1: potassium tert-butylate / tetrahydrofuran; N,N-dimethyl-formamide / 2.67 h / -78 °C

2.2: -78 - 20 °C

3.1: sodium hydroxide; water / methanol / 1 h / 20 °C / pH 12

4.1: phosphorus tribromide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Cooling with acetone-dry ice

With potassium tert-butylate; water; phosphorus tribromide; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 4128-17-0
(2E,6E)-farnesyl acetate

: 1597486-86-6
phenylsulfonyl hexaprenyl bromide

Guidance literature:: Multi-step reaction with 7 steps

1.1: salicylic acid; selenium(IV) oxide; tert.-butylhydroperoxide / water; dichloromethane / 24 h / 0 - 20 °C

2.1: sodium tetrahydroborate / methanol; tetrahydrofuran / 0.75 h / -10 °C

3.1: phosphorus tribromide / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

4.1: N,N-dimethyl-formamide / 18 h / 20 °C / Darkness

5.1: potassium tert-butylate / tetrahydrofuran; N,N-dimethyl-formamide / 2.67 h / -78 °C

5.2: -78 - 20 °C

6.1: sodium hydroxide; water / methanol / 1 h / 20 °C / pH 12

7.1: phosphorus tribromide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Cooling with acetone-dry ice

With tert.-butylhydroperoxide; selenium(IV) oxide; sodium tetrahydroborate; potassium tert-butylate; water; phosphorus tribromide; salicylic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 24163-93-7,24163-94-8,56881-57-3,6874-67-5,28290-41-7
farnesyl bromide

: 1597486-86-6
phenylsulfonyl hexaprenyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran; N,N-dimethyl-formamide / 2.67 h / -78 °C

1.2: -78 - 20 °C

2.1: sodium hydroxide; water / methanol / 1 h / 20 °C / pH 12

3.1: phosphorus tribromide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Cooling with acetone-dry ice

With potassium tert-butylate; water; phosphorus tribromide; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;