1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone

Base Information

Chemical Name:1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone
CAS No.:104324-94-9
Molecular Formula:C₁₄H₂₀O
Molecular Weight:204.312
Hs Code.:

Synonyms:1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone

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Chemical Property of 1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone

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Technology Process of 1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone

There total 2 articles about 1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 726147-66-6
1-[1-bromo-4-(4-methyl-3-pentenyl)-3-cyclohexenyl]ethan-1-one

: 104324-94-9
1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 24h;
DOI:10.1016/j.tet.2004.04.007

Reference yield:

: 123-35-3
7-methyl-3-methene-1,6-octadiene

: 78-94-4,25038-87-3
methyl vinyl ketone

: 104324-94-9
1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone

: 1-<3-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone

Guidance literature:: With thionyl chloride; diazabicyclononene; Yield given. Multistep reaction. Yields of byproduct given; 1.) reflux, 6 h; 2.) CCl₄, r.t., 2 h; 3.) toluene, reflux, 90 min;

Reference yield: 65.0%

: 917-54-4
methyllithium

: 104324-94-9
1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone

: 1-[4-methyl-4-(4-methyl-3-pentenyl)-1-cyclohexenyl]ethan-1-one

Guidance literature:: methyllithium; With copper(l) iodide; boron trifluoride diethyl etherate; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.333333h;

1-<4-(4-methyl-3-pentenyl)-1,3-cyclohexadienyl>etnanone; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h; Further stages.;
DOI:10.1016/j.tet.2004.04.007