N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide

Base Information

Chemical Name:N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide
CAS No.:79809-15-7
Molecular Formula:C₂₁H₂₇NO₆
Molecular Weight:389.448
Hs Code.:

Synonyms:N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide

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Chemical Property of N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide

Chemical Property:

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Technology Process of N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide

There total 13 articles about N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.1%

: 4697-59-0
7,8-dimethoxyisochroman-3-one

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 79809-15-7
N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide

Guidance literature:: In ethanol; for 24h; Heating;
DOI:10.1007/BF00765242

Reference yield:

: 65495-21-8
N,N-dimethyl-3,4-dimethoxybenzylamine

: 79809-15-7
N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1) n-BuLi / 1) ether, 0 deg C, 1 h; 2) 8 h

2: ethyl chloroformate, NaHCO₃ / benzene / 0.25 h

3: dimethylformamide / 20 h

4: 1) KOH; 2) HCl / 1) methanol, water, reflux, 1.5 h; 2) water, 2 h

5: 70 percent / ethanol / 4.5 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; n-butyllithium; chloroformic acid ethyl ester; sodium hydrogencarbonate; In ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4020(01)91915-5

Reference yield:

: (6-Chloromethyl-2,3-dimethoxy-phenyl)-methanol

: 79809-15-7
N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / 20 h

2: 1) KOH; 2) HCl / 1) methanol, water, reflux, 1.5 h; 2) water, 2 h

3: 70 percent / ethanol / 4.5 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)91915-5