6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate

Base Information

Chemical Name:6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate
CAS No.:1422431-12-6
Molecular Formula:C₂₃H₂₉NO₇
Molecular Weight:431.486
Hs Code.:

Synonyms:6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate

Suppliers and Price of 6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate

There total 9 articles about 6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 79809-15-7
N-<2-(3,4-dimethoxyphenyl)ethyl>(3,4-dimethoxy-2-hydroxymethyl)-phenylacetamide

: 75-36-5
acetyl chloride

: 1422431-12-6
6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 1.5h;
DOI:10.1016/j.bmc.2012.12.016

Reference yield:

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 1422431-12-6
6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: acetic acid; bromine / 2 h / 20 °C

2.1: potassium carbonate / acetone / Reflux

3.1: potassium hydroxide; water; copper; copper(II) oxide / 1 h / 140 °C / Inert atmosphere; Microwave irradiation

4.1: phenylboronic acid / toluene / 1 h / Reflux; Dean-Stark

4.2: 46 h / 100 °C / Molecular sieve; Sealed tube

4.3: 2 h / Reflux

5.1: potassium carbonate / acetone / 4 h / Reflux

6.1: ethanol / 14 h / Reflux

7.1: pyridine / dichloromethane / 1.5 h / 0 - 20 °C

With pyridine; water; bromine; copper; potassium carbonate; acetic acid; copper(II) oxide; potassium hydroxide; phenylboronic acid; In ethanol; dichloromethane; acetone; toluene;
DOI:10.1016/j.bmc.2012.12.016

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 1422431-12-6
6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; ammonium acetate / 100 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Reflux

3: ethanol / 14 h / Reflux

4: pyridine / dichloromethane / 1.5 h / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; ammonium acetate; acetic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.bmc.2012.12.016