4-chlorophenyl 1H-imidazole-1-sulfonate

Base Information

• Chemical Name: 4-chlorophenyl 1H-imidazole-1-sulfonate
• CAS No.: 1198184-09-6
• Molecular Formula: C₉H₇ClN₂O₃S
• Molecular Weight: 258.685
• Mol file: 1198184-09-6.mol

Synonyms:4-chlorophenyl 1H-imidazole-1-sulfonate

Chemical Property of 4-chlorophenyl 1H-imidazole-1-sulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-chlorophenyl 1H-imidazole-1-sulfonate

There total 1 articles about 4-chlorophenyl 1H-imidazole-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4-chloro-phenol (106-48-9,82344-39-6) + N,N`-sulfuryldiimidazole (7189-69-7) → 4-chlorophenyl 1H-imidazole-1-sulfonate (1198184-09-6)

Guidance literature:

With caesium carbonate; In tetrahydrofuran; at 20 ℃;

DOI:10.1002/adsc.201200364

Reference yield: 81.0%

4-chlorophenyl 1H-imidazole-1-sulfonate (1198184-09-6) + 5-chloro-benzoxazole (17200-29-2) → 5-chloro-2-(4-chlorophenyl)-1,3-benzoxazole (955-77-1)

Guidance literature:

With palladium diacetate; caesium carbonate; 1,2-bis-(diphenylphosphino)ethane; In 1-methyl-pyrrolidin-2-one; at 100 ℃; for 15h; Inert atmosphere;

DOI:10.1021/ol9028034

Reference yield: 79.0%

4-chlorophenyl 1H-imidazole-1-sulfonate (1198184-09-6) + acetone (67-64-1) → 1-(4-chlorophenyl)propan-2-one (5586-88-9)

Guidance literature:

With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 60 ℃; for 24h; chemoselective reaction; Inert atmosphere;

DOI:10.1002/chem.201201394

upstream raw materials:

4-chloro-phenol

N,N`-sulfuryldiimidazole

Downstream raw materials:

ethyl 2-(4-chlorophenyl)-1,3-oxazole-4-carboxylate

5-chloro-2-(4-chlorophenyl)-1,3-benzoxazole

[1,1';4',1'']terphenyl

4-methyl-p-terphenyl