4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzaldehyde

Base Information

• Chemical Name: 4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzaldehyde
• CAS No.: 1372129-90-2
• Molecular Formula: C₅₁H₄₉N₃O₃S₃
• Molecular Weight: 848.166

Synonyms:4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzaldehyde

Chemical Property of 4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzaldehyde

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Technology Process of 4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzaldehyde

There total 1 articles about 4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-(7-bromobenzo[c][1,2,5]thiadiazol-4-yl)-benzaldehyde (870485-21-5) + 5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-5'-(tri-n-butylstannyl)-2,2'-bithiophene (1372129-88-8) → 4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzaldehyde (1372129-90-2)

Guidance literature:

With bis(triphenylphosphine)palladium(II)-chloride; In tetrahydrofuran; at 75 ℃; for 4.5h; Inert atmosphere;

DOI:10.1002/adfm.201102519

Reference yield: 38.0%

4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)benzaldehyde (1372129-90-2) + cyanoacetic acid (372-09-8) → (E)-3-(4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)phenyl)-2-cyanoacrylic acid (1372129-87-7)

Guidance literature:

With ammonium acetate; In dichloromethane; acetonitrile; for 45h; Reflux;

DOI:10.1002/adfm.201102519

upstream raw materials:

4-(7-bromobenzo[c][1,2,5]thiadiazol-4-yl)-benzaldehyde

5-(N,N-bis(4-hexyloxyphenyl)-4-aminophenyl)-5'-(tri-n-butylstannyl)-2,2'-bithiophene

Downstream raw materials:

(E)-3-(4-(7-(5'-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)-2,2'-bithien-5-yl)benzo[c][1,2,5]thiadiazol-4-yl)phenyl)-2-cyanoacrylic acid

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