methyl 3-methoxy-4-{[(2S,3R,4S,5R,6R)-3,4,5-tris(acetoxy)-6-[(acetyloxy)methyl]oxan-2-yl]oxy}benzoate

Base Information

Chemical Name:methyl 3-methoxy-4-{[(2S,3R,4S,5R,6R)-3,4,5-tris(acetoxy)-6-[(acetyloxy)methyl]oxan-2-yl]oxy}benzoate
CAS No.:72500-10-8
Molecular Formula:C₂₃H₂₈O₁₃
Molecular Weight:512.468
Hs Code.:

Synonyms:methyl 3-methoxy-4-{[(2S,3R,4S,5R,6R)-3,4,5-tris(acetoxy)-6-[(acetyloxy)methyl]oxan-2-yl]oxy}benzoate

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Chemical Property of methyl 3-methoxy-4-{[(2S,3R,4S,5R,6R)-3,4,5-tris(acetoxy)-6-[(acetyloxy)methyl]oxan-2-yl]oxy}benzoate

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Technology Process of methyl 3-methoxy-4-{[(2S,3R,4S,5R,6R)-3,4,5-tris(acetoxy)-6-[(acetyloxy)methyl]oxan-2-yl]oxy}benzoate

There total 8 articles about methyl 3-methoxy-4-{[(2S,3R,4S,5R,6R)-3,4,5-tris(acetoxy)-6-[(acetyloxy)methyl]oxan-2-yl]oxy}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 74808-10-9,86520-63-0,87119-53-7,92052-29-4,121238-27-5,127061-80-7,142831-80-9
2,3,4,6-tetra-O-acetyl-d-glucopyranosyl trichloroacetimidate

: 72500-10-8
methyl 3-methoxy-4-{[(2S,3R,4S,5R,6R)-3,4,5-tris(acetoxy)-6-[(acetyloxy)methyl]oxan-2-yl]oxy}benzoate

Guidance literature:: 4-hydroxy-3-methoxybenzoic acid methyl ester; 2,3,4,6-tetra-O-acetyl-d-glucopyranosyl trichloroacetimidate; In dichloromethane; at 0 ℃; Molecular sieve; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane; for 3h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2012.09.025

Reference yield: 90.0%

: 942428-83-3
2,3,4,6-tetra-O-acetyl-D-glucopyranosyl 1-(N-phenyl)-2,2,2-trifluoroacetimidate

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 72500-10-8
methyl 3-methoxy-4-{[(2S,3R,4S,5R,6R)-3,4,5-tris(acetoxy)-6-[(acetyloxy)methyl]oxan-2-yl]oxy}benzoate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo200440r

Reference yield: 46.0%

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 92052-29-4
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl trichloroacetimidate

: 72500-10-8
methyl 3-methoxy-4-{[(2S,3R,4S,5R,6R)-3,4,5-tris(acetoxy)-6-[(acetyloxy)methyl]oxan-2-yl]oxy}benzoate

Guidance literature:: 4-hydroxy-3-methoxybenzoic acid methyl ester; 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl trichloroacetimidate; With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane; at -40 - 0 ℃; for 2h; Molecular sieve; Inert atmosphere;