benzoic acid N-tert-butyl-N'-(4-chlorobenzoyl)-N'-chloromethylhydrazide

Base Information

Chemical Name:benzoic acid N-tert-butyl-N'-(4-chlorobenzoyl)-N'-chloromethylhydrazide
CAS No.:421568-94-7
Molecular Formula:C₁₉H₂₀Cl₂N₂O₂
Molecular Weight:379.286
Hs Code.:

Synonyms:benzoic acid N-tert-butyl-N'-(4-chlorobenzoyl)-N'-chloromethylhydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoic acid N-tert-butyl-N'-(4-chlorobenzoyl)-N'-chloromethylhydrazide

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Technology Process of benzoic acid N-tert-butyl-N'-(4-chlorobenzoyl)-N'-chloromethylhydrazide

There total 2 articles about benzoic acid N-tert-butyl-N'-(4-chlorobenzoyl)-N'-chloromethylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 353759-03-2
thiocarbonic acid O-[N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazino-methyl] ester S-ethyl ester

: 421568-94-7
benzoic acid N-tert-butyl-N'-(4-chlorobenzoyl)-N'-chloromethylhydrazide

Guidance literature:: With sulfuryl dichloride; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1055/s-2002-19296

Reference yield:

: 112226-61-6
halofenozide

: 421568-94-7
benzoic acid N-tert-butyl-N'-(4-chlorobenzoyl)-N'-chloromethylhydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuOK / tetrahydrofuran / 2 h / 20 °C

1.2: 61 percent / tetrahydrofuran / 16 h / 20 °C

2.1: 88 percent / SO₂Cl₂ / CH₂Cl₂ / 1 h / 20 °C

With sulfuryl dichloride; potassium tert-butylate; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2002-19296