{2-[3-(pyridin-3-ylmethyl)ureido]-4-methoxy-6-tert-butylphenoxy}methoxymethane

Base Information

Chemical Name:{2-[3-(pyridin-3-ylmethyl)ureido]-4-methoxy-6-tert-butylphenoxy}methoxymethane
CAS No.:195314-78-4
Molecular Formula:C₂₀H₂₇N₃O₄
Molecular Weight:373.452
Hs Code.:

Synonyms:{2-[3-(pyridin-3-ylmethyl)ureido]-4-methoxy-6-tert-butylphenoxy}methoxymethane

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Chemical Property of {2-[3-(pyridin-3-ylmethyl)ureido]-4-methoxy-6-tert-butylphenoxy}methoxymethane

Chemical Property:

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Technology Process of {2-[3-(pyridin-3-ylmethyl)ureido]-4-methoxy-6-tert-butylphenoxy}methoxymethane

There total 5 articles about {2-[3-(pyridin-3-ylmethyl)ureido]-4-methoxy-6-tert-butylphenoxy}methoxymethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 3731-52-0
3-Aminomethylpyridine

: 108-20-3
di-isopropyl ether

: 32315-10-9
bis(trichloromethyl) carbonate

: 195314-33-1
3-tert-butyl-5-methoxy-2-methoxymethoxyaniline

: 195314-78-4
{2-[3-(pyridin-3-ylmethyl)ureido]-4-methoxy-6-tert-butylphenoxy}methoxymethane

Guidance literature:: With triethylamine; In dichloromethane; ethyl acetate;

Reference yield:

: 121-00-6,1341-82-8
3-tert-Butyl-4-hydroxyanisole

: 195314-78-4
{2-[3-(pyridin-3-ylmethyl)ureido]-4-methoxy-6-tert-butylphenoxy}methoxymethane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 25percent HCl, NaNO₂, 2.) NaOH / 1.) H₂O, 0 deg C, 2.) H₂O, 10 deg C, 15 min

2: 68 percent / NaH / dimethylformamide / 1 h / Ambient temperature

3: 85 percent / H₂ / 10percent Pd on carbon / methanol / 2.5 h / 2660 Torr / Ambient temperature

4: 1.) Et₃N, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C to room temperature, 30 min, 2.) CH₂Cl₂, room temperature, 1 h

With hydrogenchloride; sodium hydroxide; hydrogen; sodium hydride; triethylamine; sodium nitrite; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(98)00039-X

Reference yield:

: 2-tert-Butyl-4-methoxy-6-(4-methoxy-phenylazo)-phenol

: 195314-78-4
{2-[3-(pyridin-3-ylmethyl)ureido]-4-methoxy-6-tert-butylphenoxy}methoxymethane

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / NaH / dimethylformamide / 1 h / Ambient temperature

2: 85 percent / H₂ / 10percent Pd on carbon / methanol / 2.5 h / 2660 Torr / Ambient temperature

3: 1.) Et₃N, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C to room temperature, 30 min, 2.) CH₂Cl₂, room temperature, 1 h

With hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(98)00039-X