Pt(P(C₆H₅)3)2Cl(C₂C₆H₄NO₂)

Base Information

Chemical Name:Pt(P(C₆H₅)3)2Cl(C₂C₆H₄NO₂)
CAS No.:340756-05-0
Molecular Formula:C₄₄H₃₄ClNO₂P₂Pt
Molecular Weight:901.24
Hs Code.:

Pt(P(C<sub>6</sub>H<sub>5</sub>)3)2Cl(C<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)

Synonyms:Pt(P(C₆H₅)3)2Cl(C₂C₆H₄NO₂)

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Chemical Property of Pt(P(C₆H₅)3)2Cl(C₂C₆H₄NO₂)

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Technology Process of Pt(P(C₆H₅)3)2Cl(C₂C₆H₄NO₂)

There total 1 articles about Pt(P(C₆H₅)3)2Cl(C₂C₆H₄NO₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 10199-34-5,14056-88-3,15604-36-1
bis(triphenylphosphine)platinum(II) dichloride

: 937-31-5
(4-Nitrophenyl)acetylene

: 340756-05-0
Pt(P(C₆H₅)3)2Cl(C₂C₆H₄NO₂)

Guidance literature:: With (C₂H₅)2NH; In chloroform; refluxing a mixt. of platinum complex with alkyne and Et2NH in CHCl3 for2 h; addn. of abs. EtOH, recrystn. (CHCl3/EtOH); elem. anal.;
DOI:10.1016/S0022-328X(00)00791-9

Reference yield: 50.0%

: 340756-05-0
Pt(P(C₆H₅)3)2Cl(C₂C₆H₄NO₂)

: 38215-38-2
4,4'-diethynylbiphenyl

: 340756-01-6
NO₂C₆H₄C₂Pt(P(C₆H₅)3)2C₂(C₆H₄)2C₂H

Guidance literature:: With (CH₃CH₂)2NH; copper(l) iodide; In ethanol; chloroform; addn. of amine to a soln. of ligand in CHCl3, addn. of a soln. of platinum complex in a mixt. of CHCl3 and EtOH dropwise, stirring for 15 h at room temp.; filtration, concn., addn. od EtOH, dissolving ppt. in 1:1 mixt. of CH2Cl2 with toluene, chromy (SiO2, CH2Cl2/toluene 1:1), evapn., recrystn. (CHCl3); elem. anal.;
DOI:10.1016/S0022-328X(00)00533-7

Reference yield: 50.0%

: 340756-05-0
Pt(P(C₆H₅)3)2Cl(C₂C₆H₄NO₂)

: 38215-38-2
4,4'-diethynylbiphenyl

: 340756-01-6
NO₂C₆H₄C₂Pt(P(C₆H₅)3)2C₂(C₆H₄)2C₂H

: (NO₂C₆H₄C₂Pt(P(C₆H₅)3)2C₂C₆H₄)2

Guidance literature:: With (CH₃CH₂)2NH; In chloroform; addn. of amine to a soln. of ligand and platinum complex in CHCl3, refluxing for 48 h; concn., addn. od EtOH, dissolving ppt. in 1:1 mixt. of CH2Cl2 with toluene, column chromy (SiO2, CH2Cl2/toluene 1:1), evapn.; elem. anal.;
DOI:10.1016/S0022-328X(00)00533-7