Methyl diacetoxy-6-gingerdiol

Base Information

Chemical Name:Methyl diacetoxy-6-gingerdiol
CAS No.:863780-90-9
Molecular Formula:C₂₂H₃₄O₆
Molecular Weight:394.508
Hs Code.:

Synonyms:(3R,5S)-1-(3,4-dimethoxyphenyl)decane-3,5-diyl diacetate

Suppliers and Price of Methyl diacetoxy-6-gingerdiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
Methyldiacetoxy-6-gingerdiol ≥98%
5mg
$ 613.00

Total 7 raw suppliers

Chemical Property of Methyl diacetoxy-6-gingerdiol

Chemical Property:

Purity/Quality:

Analysis control,HPLC≥95% ^*data from raw suppliers

Methyldiacetoxy-6-gingerdiol ≥98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Methyl diacetoxy-6-gingerdiol

There total 17 articles about Methyl diacetoxy-6-gingerdiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1360109-94-9
(3R,5S)-1-(3,4-dimethoxyphenyl)decane-3,5-diol

: 108-24-7
acetic anhydride

: 863780-90-9
(3R,5S)-1-(3,4-dimethoxyphenyl)decane-3,5-diyl diacetate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.11.010

Reference yield:

: 53254-51-6,143615-75-2
(3R,5S)-1-(4-hydroxy-3-methoxyphenyl)decane-3,5-diyl diacetate

: 74-88-4
methyl iodide

: 863780-90-9
(3R,5S)-1-(3,4-dimethoxyphenyl)decane-3,5-diyl diacetate

Guidance literature:: With potassium carbonate; In acetone; Ambient temperature;
DOI:10.1016/0031-9422(92)83147-Q

Reference yield:

: 1360109-86-9
(S)-1-(4-(benzyloxy)-3-methoxyphenyl)-5-(tert-butyldimethylsilyloxy)dec-1-yn-3-one

: 863780-90-9
(3R,5S)-1-(3,4-dimethoxyphenyl)decane-3,5-diyl diacetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen; palladium(II) hydroxide / benzene / 5 h / 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere

3.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.5 h / -78 °C / Inert atmosphere

3.2: 6 h / -78 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.2: Inert atmosphere

6.1: methanol; toluene-4-sulfonic acid / 1 h / 0 - 20 °C / Inert atmosphere

7.1: dmap; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With methanol; dmap; diethyl methoxy borane; tetrabutyl ammonium fluoride; hydrogen; palladium(II) hydroxide; sodium hydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1016/j.tetasy.2011.11.010