1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline

Base Information

Chemical Name:1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline
CAS No.:86826-92-8
Molecular Formula:C₁₈H₁₄BrNO₄
Molecular Weight:388.217
Hs Code.:

Synonyms:1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline

Chemical Property:

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Technology Process of 1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline

There total 4 articles about 1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 86826-91-7
1-(2'-Bromo-5'-methoxybenzyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline

: 86826-92-8
1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline

Guidance literature:: With manganese(IV) oxide; In chloroform; for 10h;

Reference yield:

: 1798-09-0
m-methoxyphenylacetic acid

: 86826-92-8
1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / Br₂, NaOAc / acetic acid / 3 h / ice-bath

2: 87 percent / 3 h / 180 °C

3: 73 percent / POCl₃ / toluene

4: 58 percent / active MnO₂ / CHCl₃ / 10 h

With manganese(IV) oxide; bromine; sodium acetate; trichlorophosphate; In chloroform; acetic acid; toluene;

Reference yield:

: 86826-93-9
2-(2-bromo-5-methoxyphenyl)acetic acid

: 86826-92-8
1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / 3 h / 180 °C

2: 73 percent / POCl₃ / toluene

3: 58 percent / active MnO₂ / CHCl₃ / 10 h

With manganese(IV) oxide; trichlorophosphate; In chloroform; toluene;