1-(2'-Bromo-5'-methoxybenzoyl)-2-methyl-3,4-dihydro-6,7-methylenedioxyisoquinolium iodide

Base Information

Chemical Name:1-(2'-Bromo-5'-methoxybenzoyl)-2-methyl-3,4-dihydro-6,7-methylenedioxyisoquinolium iodide
CAS No.:81531-48-8
Molecular Formula:C₁₉H₁₇BrNO₄*I
Molecular Weight:530.157
Hs Code.:

Synonyms:1-(2'-Bromo-5'-methoxybenzoyl)-2-methyl-3,4-dihydro-6,7-methylenedioxyisoquinolium iodide

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Chemical Property of 1-(2'-Bromo-5'-methoxybenzoyl)-2-methyl-3,4-dihydro-6,7-methylenedioxyisoquinolium iodide

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Technology Process of 1-(2'-Bromo-5'-methoxybenzoyl)-2-methyl-3,4-dihydro-6,7-methylenedioxyisoquinolium iodide

There total 5 articles about 1-(2'-Bromo-5'-methoxybenzoyl)-2-methyl-3,4-dihydro-6,7-methylenedioxyisoquinolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 86826-92-8
1-(2'-Bromo-5'-methoxybenzoyl)-3,4-dihydro-6,7-methylenedioxyisoquinoline

: 74-88-4
methyl iodide

: 81531-48-8
1-(2'-Bromo-5'-methoxybenzoyl)-2-methyl-3,4-dihydro-6,7-methylenedioxyisoquinolium iodide

Guidance literature:: for 6h; Heating;

Reference yield:

: 1798-09-0
m-methoxyphenylacetic acid

: 81531-48-8
1-(2'-Bromo-5'-methoxybenzoyl)-2-methyl-3,4-dihydro-6,7-methylenedioxyisoquinolium iodide

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / Br₂, NaOAc / acetic acid / 3 h / ice-bath

2: 87 percent / 3 h / 180 °C

3: 73 percent / POCl₃ / toluene

4: 58 percent / active MnO₂ / CHCl₃ / 10 h

5: 95 percent / 6 h / Heating

With manganese(IV) oxide; bromine; sodium acetate; trichlorophosphate; In chloroform; acetic acid; toluene;

Reference yield:

: 86826-93-9
2-(2-bromo-5-methoxyphenyl)acetic acid

: 81531-48-8
1-(2'-Bromo-5'-methoxybenzoyl)-2-methyl-3,4-dihydro-6,7-methylenedioxyisoquinolium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / 3 h / 180 °C

2: 73 percent / POCl₃ / toluene

3: 58 percent / active MnO₂ / CHCl₃ / 10 h

4: 95 percent / 6 h / Heating

With manganese(IV) oxide; trichlorophosphate; In chloroform; toluene;