4-[1-(4-methylthiobenzyl)-5-chlorobenzimidazol-2-yl]-3,3-dimethylbutanoic acid

Base Information

Chemical Name:4-[1-(4-methylthiobenzyl)-5-chlorobenzimidazol-2-yl]-3,3-dimethylbutanoic acid
CAS No.:144727-65-1
Molecular Formula:C₂₁H₂₃ClN₂O₂S
Molecular Weight:402.945
Hs Code.:

Synonyms:4-[1-(4-methylthiobenzyl)-5-chlorobenzimidazol-2-yl]-3,3-dimethylbutanoic acid

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Chemical Property of 4-[1-(4-methylthiobenzyl)-5-chlorobenzimidazol-2-yl]-3,3-dimethylbutanoic acid

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Technology Process of 4-[1-(4-methylthiobenzyl)-5-chlorobenzimidazol-2-yl]-3,3-dimethylbutanoic acid

There total 6 articles about 4-[1-(4-methylthiobenzyl)-5-chlorobenzimidazol-2-yl]-3,3-dimethylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874-87-3
1-(chloromethyl)-4-methylthiobenzene

: 144727-65-1
4-[1-(4-methylthiobenzyl)-5-chlorobenzimidazol-2-yl]-3,3-dimethylbutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / sodium acetate, iodine / 12 h / 120 °C

2: 85 percent / H₂ / Raney nickel / tetrahydrofuran / Ambient temperature

3: triethylamine / CHCl₃ / 2 h / Ambient temperature

4: hydrochloric acid, acetic acid / H₂O / 4 h / Heating

With hydrogenchloride; hydrogen; iodine; sodium acetate; acetic acid; triethylamine; nickel; In tetrahydrofuran; chloroform; water;

Reference yield:

: 89-63-4
4-Chloro-2-nitroaniline

: 144727-65-1
4-[1-(4-methylthiobenzyl)-5-chlorobenzimidazol-2-yl]-3,3-dimethylbutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / sodium acetate, iodine / 12 h / 120 °C

2: 85 percent / H₂ / Raney nickel / tetrahydrofuran / Ambient temperature

3: triethylamine / CHCl₃ / 2 h / Ambient temperature

4: hydrochloric acid, acetic acid / H₂O / 4 h / Heating

With hydrogenchloride; hydrogen; iodine; sodium acetate; acetic acid; triethylamine; nickel; In tetrahydrofuran; chloroform; water;

Reference yield:

: 144728-05-2
(4-Chloro-2-nitro-phenyl)-(4-methylsulfanyl-benzyl)-amine

: 144727-65-1
4-[1-(4-methylthiobenzyl)-5-chlorobenzimidazol-2-yl]-3,3-dimethylbutanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / H₂ / Raney nickel / tetrahydrofuran / Ambient temperature

2: triethylamine / CHCl₃ / 2 h / Ambient temperature

3: hydrochloric acid, acetic acid / H₂O / 4 h / Heating

With hydrogenchloride; hydrogen; acetic acid; triethylamine; nickel; In tetrahydrofuran; chloroform; water;