Pyrrolidine-1-carbodithioic acid (E)-5-phenyl-1-trimethylsilanylmethyl-pent-2-enyl ester

Base Information

Chemical Name:Pyrrolidine-1-carbodithioic acid (E)-5-phenyl-1-trimethylsilanylmethyl-pent-2-enyl ester
CAS No.:86826-40-6
Molecular Formula:C₂₀H₃₁NS₂Si
Molecular Weight:377.69
Hs Code.:

Synonyms:Pyrrolidine-1-carbodithioic acid (E)-5-phenyl-1-trimethylsilanylmethyl-pent-2-enyl ester

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Chemical Property of Pyrrolidine-1-carbodithioic acid (E)-5-phenyl-1-trimethylsilanylmethyl-pent-2-enyl ester

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Technology Process of Pyrrolidine-1-carbodithioic acid (E)-5-phenyl-1-trimethylsilanylmethyl-pent-2-enyl ester

There total 4 articles about Pyrrolidine-1-carbodithioic acid (E)-5-phenyl-1-trimethylsilanylmethyl-pent-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 701-13-3
Pyrrolidine-1-carbodithioic acid allyl ester

: 86826-40-6
Pyrrolidine-1-carbodithioic acid (E)-5-phenyl-1-trimethylsilanylmethyl-pent-2-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -60 deg C

2: 2,2,4-trimethyl-pentane / Heating

3: 1.) LDA / 1.) THF, -60 deg C

With lithium diisopropyl amide; In 2,2,4-trimethylpentane;
DOI:10.1016/S0040-4039(00)87972-1

Reference yield:

: 17376-04-4
2-phenethyl iodide

: 86826-40-6
Pyrrolidine-1-carbodithioic acid (E)-5-phenyl-1-trimethylsilanylmethyl-pent-2-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -60 deg C

2: 2,2,4-trimethyl-pentane / Heating

3: 1.) LDA / 1.) THF, -60 deg C

With lithium diisopropyl amide; In 2,2,4-trimethylpentane;
DOI:10.1016/S0040-4039(00)87972-1

Reference yield:

: 86826-34-8
Pyrrolidine-1-carbodithioic acid 1-phenethyl-allyl ester

: 86826-40-6
Pyrrolidine-1-carbodithioic acid (E)-5-phenyl-1-trimethylsilanylmethyl-pent-2-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2,4-trimethyl-pentane / Heating

2: 1.) LDA / 1.) THF, -60 deg C

With lithium diisopropyl amide; In 2,2,4-trimethylpentane;
DOI:10.1016/S0040-4039(00)87972-1