benzyl 4-O-benzoyl-3-O-(2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside

Base Information

Chemical Name:benzyl 4-O-benzoyl-3-O-(2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside
CAS No.:108319-56-8
Molecular Formula:C₂₆H₃₂O₈
Molecular Weight:472.535
Hs Code.:

Synonyms:benzyl 4-O-benzoyl-3-O-(2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside

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Chemical Property of benzyl 4-O-benzoyl-3-O-(2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside

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Technology Process of benzyl 4-O-benzoyl-3-O-(2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside

There total 12 articles about benzyl 4-O-benzoyl-3-O-(2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside

: 108319-56-8
benzyl 4-O-benzoyl-3-O-(2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside

Guidance literature:: With sodium methylate;

Reference yield: 75.0%

: benzyl 4-O-benzoyl-3-O-(2-bromo-2,6-dideoxy-β-D-glucopyranosyl)-2-bromo-2,6-dideoxy-β-D-galactopyranoside

: 108319-56-8
benzyl 4-O-benzoyl-3-O-(2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1080/07328303.2017.1397682

Reference yield:

: 85726-76-7
methyl 4-O-benzoyl-2,3-O-isopropylidene-α-D-rhamnopyranoside

: 108319-56-8
benzyl 4-O-benzoyl-3-O-(2,6-dideoxy-3-O-formyl-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / Br₂CHOCH₃ / ZnBr₂

2: AgOSO₂CF₃

3: 76 percent / (C₄H₉)3SnH

4: 78 percent / CH₃ONa

With α,α-dibromomethyl methyl ether; tri-n-butyl-tin hydride; sodium methylate; silver trifluoromethanesulfonate; zinc dibromide;