[3-Ethoxycarbonylmethoxy-5-(1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carbonyl)-phenoxy]-acetic acid ethyl ester; hydrochloride

Base Information

Chemical Name:[3-Ethoxycarbonylmethoxy-5-(1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carbonyl)-phenoxy]-acetic acid ethyl ester; hydrochloride
CAS No.:142109-57-7
Molecular Formula:C₂₇H₄₂N₂O₁₁*ClH
Molecular Weight:607.098
Hs Code.:

Synonyms:[3-Ethoxycarbonylmethoxy-5-(1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carbonyl)-phenoxy]-acetic acid ethyl ester; hydrochloride

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Chemical Property of [3-Ethoxycarbonylmethoxy-5-(1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carbonyl)-phenoxy]-acetic acid ethyl ester; hydrochloride

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Technology Process of [3-Ethoxycarbonylmethoxy-5-(1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carbonyl)-phenoxy]-acetic acid ethyl ester; hydrochloride

There total 5 articles about [3-Ethoxycarbonylmethoxy-5-(1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carbonyl)-phenoxy]-acetic acid ethyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 141810-49-3
16-(3,5-Bis-ethoxycarbonylmethoxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carboxylic acid benzyl ester

: 142109-57-7
[3-Ethoxycarbonylmethoxy-5-(1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carbonyl)-phenoxy]-acetic acid ethyl ester; hydrochloride

Guidance literature:: With hydrogen; hydrochloric acid 1,4-dioxane; palladium on activated charcoal; In ethanol;
DOI:10.1039/c39920000608

Reference yield:

: 42031-79-8
7-(Benzyloxycarbonyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecan

: 142109-57-7
[3-Ethoxycarbonylmethoxy-5-(1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carbonyl)-phenoxy]-acetic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / NEt₃ / benzene

2: 87 percent / NaOH / methanol; H₂O

3: 48 percent / K₂CO₃ / acetone

4: 87 percent / H₂, HCl*dioxane / Pd/C / ethanol

With sodium hydroxide; hydrogen; potassium carbonate; triethylamine; hydrochloric acid 1,4-dioxane; palladium on activated charcoal; In methanol; ethanol; water; acetone; benzene;
DOI:10.1039/c39920000608

Reference yield:

: 39192-49-9
3,5-diacetoxybenzoyl chloride

: 142109-57-7
[3-Ethoxycarbonylmethoxy-5-(1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane-7-carbonyl)-phenoxy]-acetic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / NEt₃ / benzene

2: 87 percent / NaOH / methanol; H₂O

3: 48 percent / K₂CO₃ / acetone

4: 87 percent / H₂, HCl*dioxane / Pd/C / ethanol

With sodium hydroxide; hydrogen; potassium carbonate; triethylamine; hydrochloric acid 1,4-dioxane; palladium on activated charcoal; In methanol; ethanol; water; acetone; benzene;
DOI:10.1039/c39920000608