benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate)

Base Information

Chemical Name:benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate)
CAS No.:1620482-22-5
Molecular Formula:C₁₂H₄F₆O₆S₄
Molecular Weight:486.415
Hs Code.:

Synonyms:benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate)

Suppliers and Price of benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate)

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate)

There total 2 articles about benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1357156-35-4
4,8-dihydroxybenzo[1,2-b:4,5-b']dithiophene

: 1620482-22-5
benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate)

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c4tc02107j

Reference yield:

: 32281-36-0
4,8-dihydrobenzo[1,2-b:4,5-b']dithiophene-4,8-dione

: 1620482-22-5
benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 12 h / 85 °C / Cooling with ice

2: pyridine / dichloromethane / 12 h / 0 °C

With pyridine; sodium tetrahydroborate; In ethanol; dichloromethane;
DOI:10.1039/c4ta01226g

Reference yield: 90.0%

: 1620482-22-5
benzo[1,2-b:4,5-b']dithiophene-4,8-diyl bis(trifluoromethanesulfonate)

: 98-80-6
phenylboronic acid

: 1574548-65-4
4,8-diphenylbenzo[1,2-b:4,5-b’]dithiophene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; at 85 ℃; for 16h;
DOI:10.1039/c4ta01226g