1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose

Base Information

Chemical Name:1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose
CAS No.:153915-03-8
Molecular Formula:C₂₄H₂₃N₃O₉
Molecular Weight:497.461
Hs Code.:

Synonyms:1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose

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Chemical Property of 1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose

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Technology Process of 1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose

There total 2 articles about 1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153914-98-8
3-Azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

: 153915-03-8
1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: aq. AcOH

2: pyridine

With pyridine; acetic acid;
DOI:10.1039/b005469k

Reference yield:

: 108-24-7
acetic anhydride

: C₂₀H₁₉N₃O₇

: 153915-03-8
1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose

Guidance literature:: With pyridine;
DOI:10.1039/b005469k

Reference yield: 68.0%

: 65-71-4,28806-14-6,691841-57-3
thymin

: 153915-03-8
1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose

: 319919-34-1
1-(2-O-Acetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-β-D-erythro-pentofuranosyl)thymine

Guidance literature:: thymin; 1,2-O-Diacetyl-3-azido-5-O-benzoyl-4-C-benzoyloxymethyl-3-deoxy-D-erythro-pentofuranose; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; for 1h; Heating;

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 60 ℃; for 16.1667h;
DOI:10.1039/b005469k