Technology Process of 2-(2-bromoethyl)-6-methylanisole
There total 5 articles about 2-(2-bromoethyl)-6-methylanisole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
carbon tetrabromide; triphenylphosphine;
In
dichloromethane;
at 20 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 90 percent / benzyltriethylammonium bromide; aq. KOH / CH2Cl2 / 24 h / 20 °C
2.1: O3; O2 / methanol / 0.2 h / -90 °C
2.2: 97 percent / NaBH4 / methanol / -50 - 20 °C
3.1: 93 percent / CBr4; PPh3 / CH2Cl2 / 20 h / 20 °C
With
potassium hydroxide; carbon tetrabromide; oxygen; benzyltriethylammonium bromide; ozone; triphenylphosphine;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Heating
2.1: 90 percent / benzyltriethylammonium bromide; aq. KOH / CH2Cl2 / 24 h / 20 °C
3.1: O3; O2 / methanol / 0.2 h / -90 °C
3.2: 97 percent / NaBH4 / methanol / -50 - 20 °C
4.1: 93 percent / CBr4; PPh3 / CH2Cl2 / 20 h / 20 °C
With
potassium hydroxide; carbon tetrabromide; oxygen; benzyltriethylammonium bromide; ozone; triphenylphosphine;
In
methanol; dichloromethane;
1.1: Claisen rearrangement;