[5,15-bis(ethynyl)-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc

Base Information

• Chemical Name: [5,15-bis(ethynyl)-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc
• CAS No.: 1200931-08-3
• Molecular Formula: C₈₄H₁₁₆N₄O₄Zn
• Molecular Weight: 1311.26
• Mol file: 1200931-08-3.mol

Synonyms:[5,15-bis(ethynyl)-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc

Chemical Property of [5,15-bis(ethynyl)-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of [5,15-bis(ethynyl)-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc

There total 2 articles about [5,15-bis(ethynyl)-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C102H156N4O4Si2Zn → [5,15-bis(ethynyl)-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc (1200931-08-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/jccs.201900158

Reference yield:

[5,15-bis-[(trimethylsilanyl)ethynyl]-10,20-bis[2,6-di(dodecyloxy)phenyl]porphynato]zinc → [5,15-bis(ethynyl)-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc (1200931-08-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1021/la9031927

Reference yield: 55.0%

4-iodobenzoic acid (619-58-9) + [5,15-bis(ethynyl)-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc (1200931-08-3) + 2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-8-(4-iodophenyl)-4-bora-3a,4a-diaza-s-indacene → C114H147BF2N6O6Zn

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; triethylamine; triphenylphosphine; In toluene; at 20 ℃; for 12.1667h; Inert atmosphere;

DOI:10.1021/la9031927

Downstream raw materials:

[5-ethynyl-15-(trihexylsilanyl)ethynyl-10,20-bis[2,6-di(dodecyloxy)phenyl]porphinato]zinc