anhydro 7-phenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxide

Base Information

• Chemical Name: anhydro 7-phenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxide
• CAS No.: 95113-05-6
• Molecular Formula: C₁₁H₁₁N₅S₂
• Molecular Weight: 277.374

Synonyms:anhydro 7-phenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxide

Chemical Property of anhydro 7-phenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxide

Chemical Property:

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Technology Process of anhydro 7-phenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxide

There total 2 articles about anhydro 7-phenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

phenyl isothiocyanate (103-72-0) + 4-Amino-1-methyl-bis-1,2,4-triazolium iodide (86663-28-7) → anhydro 7-phenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxide (95113-05-6)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 6h; Ambient temperature; Irradiation; ultrasound;

DOI:10.1016/S0040-4020(01)87630-4

Reference yield:

7-phenyl-1-methyl-3,6-bis(methylthio)1.2.4-triazolo<4,3-b>-1,2,4-triazolium iodide → anhydro 7-phenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxide (95113-05-6)

Guidance literature:

In benzene; Product distribution; Heating;

DOI:10.1016/S0040-4039(01)91302-4

Reference yield: 78.0%

anhydro 7-phenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxide (95113-05-6) + methyl iodide (74-88-4) → 7-phenyl-1-methyl-3,6-bis(methylthio)1.2.4-triazolo<4,3-b>-1,2,4-triazolium iodide

Guidance literature:

In benzene; for 24h; Ambient temperature;

DOI:10.1016/S0040-4020(01)87630-4

upstream raw materials:

phenyl isothiocyanate

4-Amino-1-methyl-bis-1,2,4-triazolium iodide

Downstream raw materials:

(2-Methyl-5-methylsulfanyl-2H-[1,2,4]triazol-3-yl)-phenyl-cyanamide

1-(5-Dicyanomethylene-1-methyl-3-methylsulfanyl-1,5-dihydro-[1,2,4]triazol-4-yl)-2-methyl-3-phenyl-isothiourea

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